Facile Green Synthesis of LaCe Co-Doped ZnO Nanoparticles and Their Structural, Optical and Antibacterial Properties

M. Karthikeyan, A. Ahamed, P. Kumar
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引用次数: 3

Abstract

This present work describes the synthesis of LaCe co-doped zinc oxide (ZnO) nanoparticles (NPs) prepared by green method using Gymnema sylvestre (G. sylvestre) leaves as reducing as well as capping agent. Green synthesis method avoids inert gases, high pressure, laser radiation, high temperature, toxic chemicals etc. as compared to conventional method like sol-gel technique method, laser ablation method, solvothermal method, inert gas condensation method and chemical reduction method. The synthesized LaCe co-doped ZnO NPs was characterized by X-Ray diffraction (XRD), field emission scanning electron microscopy (FESEM), elemental analysis (EADX), Fourier transform infrared spectroscopy (FTIR), UV-vis spectroscopy and photoluminescence (PL). The LaCe co-doped ZnO NPs was tested against clinical pathogens such as gram positive G+ (Staphylococcus aureus and Streptococcus pneumoniae) and gram negative G- (Klebsiella pneumoniae, Shigella sydenteriae, Escherichia coli, Pseudomonas aeruginosa and Protus vulgaris) bacterial strains using agar well diffusion method.
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LaCe共掺杂ZnO纳米粒子的绿色合成及其结构、光学和抗菌性能
本工作描述了用绿化法合成LaCe共掺杂氧化锌纳米粒子(NPs),该纳米粒子以匙羹藤(G. sylvestre)叶子为还原剂和封盖剂。与溶胶-凝胶法、激光烧蚀法、溶剂热法、惰性气体冷凝法、化学还原法等传统合成方法相比,绿色合成方法避免了惰性气体、高压、激光辐射、高温、有毒化学品等。采用x射线衍射(XRD)、场发射扫描电镜(FESEM)、元素分析(EADX)、傅里叶变换红外光谱(FTIR)、紫外可见光谱(UV-vis)和光致发光(PL)对合成的LaCe共掺杂ZnO NPs进行了表征。采用琼脂孔扩散法检测LaCe共掺杂ZnO NPs对革兰氏阳性G+(金黄色葡萄球菌和肺炎链球菌)和革兰氏阴性G-(肺炎克雷伯氏菌、西肠志贺氏菌、大肠埃希菌、铜绿假单胞菌和寻常原菌)菌株的临床致病菌的抑制作用。
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