{"title":"Optimization of synthesis conditions for CoSb3 compounds prepared by Sb self-flux method","authors":"T. Souma, M. Ohtaki","doi":"10.1109/ICT.2006.331385","DOIUrl":null,"url":null,"abstract":"CoSb3 bulk materials were successfully prepared by Sb self-flux technique, and the synthesis conditions were widely investigated to obtain the high purity compounds utilizing a quantitative powder XRD study with the Rietveld analysis applying a multi-phase-fitting condition. The reaction temperature range for the Sb self-flux technique was extended up to 1123 K to promote the reaction in the Co-Sb system. The relation between the reaction temperature and the chemical composition is discussed to optimize the preparation conditions in the Sb self-flux technique","PeriodicalId":346555,"journal":{"name":"2006 25th International Conference on Thermoelectrics","volume":"1 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2006-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"2006 25th International Conference on Thermoelectrics","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1109/ICT.2006.331385","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
CoSb3 bulk materials were successfully prepared by Sb self-flux technique, and the synthesis conditions were widely investigated to obtain the high purity compounds utilizing a quantitative powder XRD study with the Rietveld analysis applying a multi-phase-fitting condition. The reaction temperature range for the Sb self-flux technique was extended up to 1123 K to promote the reaction in the Co-Sb system. The relation between the reaction temperature and the chemical composition is discussed to optimize the preparation conditions in the Sb self-flux technique
京公网安备 11010802042870号
京ICP备2023020795号-1
分享
求助内容：
应助结果提醒方式：
扫码关注我们
