Low temperature synthesis of carbon nanotubes and carbon nanospheres

M. G. Kibria, A. K. M. Bazlur Rashid
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引用次数: 1

Abstract

Recently nanomaterial have gained a great interest due to their unique electrical and optical properties. The area of carbon materials have since been dominated by studies of carbon nanotubes. So far numerous methods have been developed for the synthesis of CNTs; in this work we have synthesized CNTs via a simple chemical route. Carbon nanotubes (CNTs) are successfully synthesized by heating a mixture of ferrocene and ammonium chloride at temperature as low as 250 °C. Carbon nanospheres are also observed here. Carbon spheres (CSs) of different sizes and shapes are present randomly in the sample. Field emission scanning electron microscopy is performed to examine the morphology of the sample and Energy Dispersive X-ray Spectroscopy (EDX) is performed to examine the composition.
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碳纳米管和碳纳米球的低温合成
近年来,纳米材料以其独特的电学和光学特性引起了人们的极大兴趣。碳材料的研究一直以碳纳米管的研究为主。到目前为止,已经开发了许多合成碳纳米管的方法;在这项工作中,我们通过简单的化学途径合成了碳纳米管。采用低至250℃的温度加热二茂铁和氯化铵的混合物,成功合成了碳纳米管。这里也观察到碳纳米球。不同大小和形状的碳球(CSs)在样品中随机存在。用场发射扫描电子显微镜检查样品的形貌,用能量色散x射线光谱学(EDX)检查其组成。
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