A Specific and Sensitive Method for the Quantitative Determination of Nitrite

Kunio Suzuki, T. Mitsuoka
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引用次数: 1

Abstract

A specific and sensitive method was established for the determination of nitrite in biological materials. In the first step, nitrite is converted with diethylamine into N-nitrosodiethylamine by the N-nitrosation reaction under acidic condition. In the second step, the N-nitrosodiethylamine is determined by gas-liquid chromatography connected to a thermal energy analyzer (GC-TEA) . This method is effective and practical.
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一种特异灵敏的亚硝酸盐定量测定方法
建立了一种特异、灵敏的测定生物材料中亚硝酸盐的方法。第一步,在酸性条件下,亚硝酸盐与二乙胺通过n -亚硝化反应转化为n -亚硝基二乙胺。第二步,n -亚硝基二乙胺通过气液色谱法与热能分析仪(GC-TEA)相连接进行测定。该方法有效实用。
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