IN SITU TIME RESOLVED LAUE DIFFRACTION DURING MICRO-COMPRESSION EXPERIMENTS

R. Maaß, S. Petegem, H. Swygenhoven, D. Grolimund, P. Derlet, C. Volkert
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Abstract

We present in situ and ex situ Laue micro-diffraction experiments on micron-sized single crystal pillars. We show that the focused ion beam technique introduces measurable damage in Si pillars. The dynamics of the Laue patterns of Au pillars demonstrate the occurrence of crystal rotation and strengthening is explained by plasticity starting on a slip system that is geometrically not predicted but selected because of the character of the pre-existing strain gradient.
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微压缩实验中现场时间分辨劳厄衍射
本文对微米级单晶柱进行了原位和非原位劳厄微衍射实验。我们证明了聚焦离子束技术在硅柱中引入了可测量的损伤。金柱的劳厄模式的动力学表明,晶体旋转和强化的发生是由塑性开始的滑移系统来解释的,这种滑移系统在几何上是不可预测的,但由于预先存在的应变梯度的特征而被选择。
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