An alternate acid cleaning process for the regeneration of waste engine oil and a proposed procedure for the disposal of produced sludge

IF 0.1 Q4 ENGINEERING, CHEMICAL Journal of the Pakistan Institute of Chemical Engineers Pub Date : 2023-08-28 DOI:10.54693/piche.05116
Muhammad Hamza Naeem, Naseer Ahmed Khan, Naveed Ul Hasan Syed, None Saira bano, None Muddasar habib
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Abstract

In Pakistan most of the used motor oil cleaning businesses is carried out in processing containers. They do the simple heating and after that a concentrated sulphuric acid is slowly mixed at a room temperature for the removal of the oxidized carbonized substances and other dirt stuff. This study is an attempt to propose an alternate relatively cleaner methodology for the cleaning of used lubricating oil. Briefly, the spent oil was heated till the knocking sound disappeared or in other words the water is fist removed. After that at a room temperature the dehydrated oil was treated with the glacial acetic acid (instead of sulphuric acid) for an hour. A settling time of 24 hours is provided after which reddish brownish (top) and black (bottom) layers were formed. The collected upper layer was then treated with fuller earth (Multani meti) under continuous stirring. Finally, after cooling to a room temperature the oil was filtered to a reasonably regenerated lubricating oil. This cleaning process recovers about 53% v/v of the lubricating oil. The remaining sludge containing the acetic acid is a biodegradable mixture. Moreover, the sludge of the acid treatment can be mixed with cement to prepare concrete blocks.
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一种用于再生废机油的替代酸清洗工艺和一种用于处理产生的污泥的拟议程序
在巴基斯坦,大多数旧机油清洗业务是在加工容器中进行的。他们先进行简单的加热,然后将浓硫酸在室温下缓慢混合,以去除氧化、碳化的物质和其他污垢。本研究试图提出一种相对清洁的方法来清洗用过的润滑油。简单地说,将废油加热,直到敲击声消失,或者换句话说,首先将水除去。然后在室温下用冰醋酸(而不是硫酸)处理脱水油一小时。沉淀时间为24小时,之后形成红棕色(上)层和黑色(下)层。收集的上层在连续搅拌的条件下用更厚的土处理。最后,在冷却到室温后,将油过滤成合理再生的润滑油。该清洗过程回收约53% v/v的润滑油。剩余的含有乙酸的污泥是一种可生物降解的混合物。此外,酸处理后的污泥可与水泥混合配制混凝土砌块。
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