CARACTERIZAÇÃO MORFOLÓGICA DE MICROFIBRAS ELETROFIADAS DE POLIESTIRENO

Beatriz Marques Carvalho, Gabriel da Cruz Dias, Luz Marina Andrade Maruoka, Rosane Freire Boina, Deuber Lincon da Silva Agostini
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Abstract

Since wastewater treatment is of great interest to society, it is important to develop techniques that perform this treatment by removing pollutants such as dyes, pesticides, and metals. In this context, adsorption stands out as a promising method in the treatment of effluents, allied to this, as polymeric membranes considerably improve the ability to remove pollutants. Carbon-based additives, such as graphene oxide, have been used in the area of adsorption because they are an adsorbent capable of removing metallic ions and dyes. Thus, it is interesting to carry out studies of the polystyrene polymer with graphene oxide, aiming at the production of adsorbent membranes. To this end, the production of polystyrene was first analyzed, with graphene oxide added to the polymer matrix in the future. Thus, polystyrene microfibers were produced using the electrospinning technique and analyzed morphologically using optical microscopy and scanning electron microscopy (SEM). With the help of ImageJ and OriginPro 8.5 software, a histogram of the frequency distribution of microfiber diameters and the normal curve was created. Through the results obtained, it was observed that there was the production of microfibers with considerable morphology, as fibers with beads and agglomerates were not observed.. From the histogram, it was noted that the microfibers had an average diameter of 5.73 µm.
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聚苯乙烯静电纺丝微纤维的形态表征
由于废水处理引起了社会的极大兴趣,因此开发通过去除染料、农药和金属等污染物来进行废水处理的技术非常重要。在这种情况下,吸附作为一种有前途的污水处理方法脱颖而出,与此相关,因为聚合物膜大大提高了去除污染物的能力。碳基添加剂,如氧化石墨烯,已被用于吸附领域,因为它们是一种能够去除金属离子和染料的吸附剂。因此,对聚苯乙烯聚合物与氧化石墨烯进行研究,以生产吸附剂膜是很有趣的。为此,首先分析了聚苯乙烯的生产,未来将在聚合物基体中加入氧化石墨烯。利用静电纺丝技术制备了聚苯乙烯微纤维,并用光学显微镜和扫描电镜对其进行了形貌分析。利用ImageJ和OriginPro 8.5软件,绘制了微纤维直径频率分布的直方图和正态曲线。通过获得的结果,可以观察到有相当形态的微纤维的产生,因为没有观察到带有珠状和团块的纤维。从直方图中可以看出,微纤维的平均直径为5.73µm。
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发文量
17
审稿时长
12 weeks
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