14C PREPARATION PROTOCOLS FOR ARCHAEOLOGICAL SAMPLES AT THE LMC14, SACLAY, FRANCE

Abstract

The Laboratoire de Mesure du Carbone 14 (LMC14) has operated a radiocarbon dating laboratory for almost twenty years with ARTEMIS, the Accelerator Mass Spectrometer (AMS) based on a NEC 9SDH-2 Pelletron tandem accelerator. A first status report describing the chemical pretreatment methods was published in 2017 (Dumoulin et al. 2017). This article summarizes updates of the routine procedures and presents new protocols. The quality checks in place at the LMC14 and results obtained for the GIRI international inter-comparison are reported. New protocols developed by the laboratory over the last five years are described with the preparation of iron, lead white, cellulose, calcium oxalate, and mortar. This report also provides a summary of practical information for sample preparation and can help the laboratory users who provide samples and publish results to better understand all the work behind a 14C dating.