A comprehensive study on reference material of Imidacloprid in tomato matrix

Trang Nguyen Linh, Trang Tran Thi Thu, Anh Dinh Hoang, Nguyen Nguyen Thi Thao, Hong Ha Tran Thi, Hang Do Thi Thu, Phuong Kieu Thi Lan, Cuong Dang Huu, Ket Dang Van, Huyen Nguyen Thi, Thao Le Thi Phuong, Hao Le Thi Hong, Huong Nguyen Thi Anh, Hoa Nguyen Thi Minh
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Abstract

Controlling the level of crop protection chemical residues in food is always a matter of concern. Certified reference materials (CRM) or reference materials (RM) are used in crop protection chemical residue analysis to validate analytical methods and evaluate the quality of measurement results. Imidacloprid is a common crop protection chemical used in tomato crops. A comprehensive study of the production, storage, transport, and utilization of CRM imidacloprid in tomato matrix was conducted. After comparing the two frozen and freeze-dried production processes, the freeze-dried production process was concluded to be superior. The CRM characterization process complies with ISO 17034:2016. The concentration of imidacloprid in tomato CRM is consistent with the maximum residue limit of imidacloprid according to the Codex and regulations of Circular 50/2016/TT-BYT of the Ministry of Health of Vietnam. At 4°C storage temperatures, freeze-dried tomato CRM was predicted to be stable for at least 552 days, while at -20°C the shelf life was at least 704 days.
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番茄基质中吡虫啉参考物质的综合研究
控制食品中的作物保护化学品残留水平一直是人们关注的问题。农作物保护化学品残留分析中使用有证标准物质(CRM)或标准物质(RM)来验证分析方法和评估测量结果的质量。吡虫啉是番茄作物中常用的作物保护化学品。对番茄基质中 CRM 吡虫啉的生产、储存、运输和利用进行了全面研究。在对冷冻和冻干两种生产工艺进行比较后,得出冻干生产工艺更优的结论。CRM 表征过程符合 ISO 17034:2016 标准。番茄 CRM 中吡虫啉的浓度符合食品法典和越南卫生部第 50/2016/TT-BYT 号通告规定的吡虫啉最大残留限量。据预测,在 4°C 的储存温度下,冻干番茄 CRM 的稳定期至少为 552 天,而在 -20°C 的储存温度下,保质期至少为 704 天。
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