Structure and Properties of High-Speed Steel Surfaised Layer Irradiated by Pulsed Electron Beam

Yu. F. Ivanov, V. E. Gromov, T. P. Guseva, A. S. Chapaikin, E. S. Vashchuk, D. A. Romanov
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Abstract

The methods of light, scanning, and transmission electron microscopy are used to study the structure, phase composition, and properties of multilayer plasma surfacings made of high-speed steel R18YU in a protective-alloying nitrogen medium, followed by a fourfold high-temperature tempering and additional electron beam processing. After tempering, the deposited layer on the 30KHGSA high-speed steel R18YU has a polycrystalline structure with a cell size of 7–22.5 µm with layers of the second phase along the boundaries and at the joints of the grains. It is shown that the irradiation of surfaised layers with a pulsed electron beam (energy density 30 J/cm2, pulse duration 50 µs, number of pulses 5, and pulse repetition rate 0.3 s–1) leads to the formation of a thin (30–50 µm) surface layer with a cellular crystallization structure. The volume of grains is formed by a solid solution based on α-Fe. Nanoscale (10–45 nm) particles of iron, chromium, and tungsten carbides of complex composition, such as M6C and M23C6, are located in the volume and along the boundaries of the crystallization cells. Fragmentation of the surface layer by a grid of microcracks is revealed, indicating relaxation of thermal stresses formed during high-speed cooling after electron beam processing. The particles have a faceted or globular shape. After irradiation with an electron beam, the wear resistance of the material increases by more than 3 times, while maintaining the microhardness of the modified layer (~5.3 GPa).

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经脉冲电子束辐照的高速钢保护层的结构和特性
摘要 采用光电子显微镜、扫描电子显微镜和透射电子显微镜方法,研究了高速钢 R18YU 在保护合金化氮介质中经过四次高温回火和附加电子束加工制成的多层等离子表面涂层的结构、相组成和性能。回火后,30KHGSA 高速钢 R18YU 上的沉积层具有多晶结构,晶胞尺寸为 7-22.5 µm,晶粒边界和接缝处有第二相层。实验表明,用脉冲电子束(能量密度 30 J/cm2,脉冲持续时间 50 µs,脉冲数 5,脉冲重复率 0.3 s-1)辐照表面化层,可形成具有蜂窝状结晶结构的薄表层(30-50 µm)。晶粒体积由基于 α-Fe 的固溶体形成。在结晶单元的体积内和边界上分布着成分复杂的铁、铬和碳化钨的纳米级(10-45 nm)颗粒,如 M6C 和 M23C6。表面层出现网格状的微裂纹,表明电子束加工后高速冷却过程中形成的热应力发生了松弛。颗粒的形状为面状或球状。经过电子束辐照后,材料的耐磨性提高了 3 倍以上,同时还保持了改性层的显微硬度(约 5.3 GPa)。
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来源期刊
CiteScore
0.90
自引率
25.00%
发文量
144
审稿时长
3-8 weeks
期刊介绍: Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques publishes original articles on the topical problems of solid-state physics, materials science, experimental techniques, condensed media, nanostructures, surfaces of thin films, and phase boundaries: geometric and energetical structures of surfaces, the methods of computer simulations; physical and chemical properties and their changes upon radiation and other treatments; the methods of studies of films and surface layers of crystals (XRD, XPS, synchrotron radiation, neutron and electron diffraction, electron microscopic, scanning tunneling microscopic, atomic force microscopic studies, and other methods that provide data on the surfaces and thin films). Articles related to the methods and technics of structure studies are the focus of the journal. The journal accepts manuscripts of regular articles and reviews in English or Russian language from authors of all countries. All manuscripts are peer-reviewed.
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