Experimental evaluation of ZnO nanorods based eco – friendly sensor for melamine detection in milk

IF 17.7 1区 化学 Q1 CHEMISTRY, MULTIDISCIPLINARY Accounts of Chemical Research Pub Date : 2024-05-27 DOI:10.1108/sr-10-2023-0505
S. Venkatachalapathi, Radha Shankararajan, Kiruthika Ramany, Iyappan Gunasekaran
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Abstract

Purpose The purpose of this study is to develop a straightforward method for creating a non – toxic metal oxide sensor capable of detecting melamine in milk at ambient temperature. Design/methodology/approach A low temperature, straightforward solution-based approach, specifically the hydrothermal method was utilized to apply the active sensing layer onto the substrate. Subsequently, analysis of the cyclic voltammetry (CV) profile was conducted to detect the concentration of melamine and determine its sensitivity. Findings An experimental analysis was performed on a nontoxic metal oxide-based sensor fabricated for detecting melamine sensitivity using the CV profile. The sensor’s performance was evaluated under three different concentrations of melamine (0.1 mmol, 0.2 mmol and 0.3 mmol). The results demonstrated a satisfactory sensitivity of 0.0297 µAmM−1cm−2 with a response time of 2 s. Originality/value The primary innovation of this research lies in the creation of a nontoxic and environmentally friendly sensor. The synthesis method employed featured significantly lower temperatures compared to existing literatures. Furthermore, the sensor achieved enhanced sensitivity along with rapid response times.
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基于氧化锌纳米棒的牛奶中三聚氰胺生态友好型传感器的实验评估
本研究的目的是开发一种简单易行的方法,用于制造一种能够在环境温度下检测牛奶中三聚氰胺含量的无毒金属氧化物传感器。设计/方法/途径利用一种低温、简单易行的基于溶液的方法,特别是水热法,将活性传感层涂在基底上。随后,对循环伏安法(CV)曲线进行了分析,以检测三聚氰胺的浓度并确定其灵敏度。研究结果对利用循环伏安法曲线制作的无毒金属氧化物传感器进行了实验分析,以检测三聚氰胺的灵敏度。在三种不同浓度的三聚氰胺(0.1 毫摩尔、0.2 毫摩尔和 0.3 毫摩尔)条件下对传感器的性能进行了评估。结果表明,该传感器的灵敏度为 0.0297 µAmM-1cm-2,响应时间为 2 秒,令人满意。与现有文献相比,所采用的合成方法大大降低了温度。此外,该传感器还具有更高的灵敏度和更快的响应时间。
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来源期刊
Accounts of Chemical Research
Accounts of Chemical Research 化学-化学综合
CiteScore
31.40
自引率
1.10%
发文量
312
审稿时长
2 months
期刊介绍: Accounts of Chemical Research presents short, concise and critical articles offering easy-to-read overviews of basic research and applications in all areas of chemistry and biochemistry. These short reviews focus on research from the author’s own laboratory and are designed to teach the reader about a research project. In addition, Accounts of Chemical Research publishes commentaries that give an informed opinion on a current research problem. Special Issues online are devoted to a single topic of unusual activity and significance. Accounts of Chemical Research replaces the traditional article abstract with an article "Conspectus." These entries synopsize the research affording the reader a closer look at the content and significance of an article. Through this provision of a more detailed description of the article contents, the Conspectus enhances the article's discoverability by search engines and the exposure for the research.
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