An Analytical Model to Evaluate the Volumetric Strain in a Polymeric Material Using Terahertz Time-Domain Spectroscopy

IF 2.6 3区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Journal of Nondestructive Evaluation Pub Date : 2024-06-07 DOI:10.1007/s10921-024-01095-4
Sushrut Karmarkar, Mahavir Singh, Vikas Tomar
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Abstract

This work develops a polarization-dependent analytical model using terahertz time-domain spectroscopy (THz-TDS) for computing strain in materials. The model establishes a correlation between volumetric strain and the change in time of arrival for a THz pulse by using the dielectrostrictive properties, variations in doping particle density, and changes in the thickness of the sample resulting from Poisson’s effects. The analytical model is validated through strain mapping of polydimethylsiloxane (PDMS) doped with passive highly dielectrostrictive strontium titanate (STO). Two experiments, using an open-hole tensile and a circular edge-notch specimen are conducted to show the efficacy of the proposed. The stress relaxation behavior of the composite is measured and accounted for to prevent changes in strain during the measurement window. The THz strain mapping results are compared with the finite element model (FEM) and surface strain measurements using the digital image correlation (DIC) method. The experimental findings exhibit sensitivity to material features such as particle clumping and edge effects. The THz strain map shows a strong agreement with FEM and DIC results, thus demonstrating the applicability of this technique for surface and sub-surface strain mapping in polymeric composites.

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利用太赫兹时域光谱评估聚合物材料体积应变的分析模型
这项研究利用太赫兹时域光谱(THz-TDS)建立了一个偏振相关分析模型,用于计算材料中的应变。该模型利用介电致伸缩特性、掺杂颗粒密度的变化以及泊松效应导致的样品厚度变化,建立了体积应变与太赫兹脉冲到达时间变化之间的相关性。通过对掺杂了无源高介电致伸缩性钛酸锶(STO)的聚二甲基硅氧烷(PDMS)进行应变绘图,验证了该分析模型。使用开孔拉伸试样和圆形边缘缺口试样进行了两次实验,以显示所提方法的有效性。对复合材料的应力松弛行为进行了测量和计算,以防止测量窗口期间的应变变化。太赫兹应变绘图结果与有限元模型(FEM)和使用数字图像相关(DIC)方法进行的表面应变测量结果进行了比较。实验结果显示了对材料特征的敏感性,如颗粒团聚和边缘效应。太赫兹应变图与有限元模型和数字图像相关法的结果非常吻合,从而证明了该技术在聚合物复合材料表面和次表面应变图绘制中的适用性。
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来源期刊
Journal of Nondestructive Evaluation
Journal of Nondestructive Evaluation 工程技术-材料科学:表征与测试
CiteScore
4.90
自引率
7.10%
发文量
67
审稿时长
9 months
期刊介绍: Journal of Nondestructive Evaluation provides a forum for the broad range of scientific and engineering activities involved in developing a quantitative nondestructive evaluation (NDE) capability. This interdisciplinary journal publishes papers on the development of new equipment, analyses, and approaches to nondestructive measurements.
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