Strength evolution and deterioration law of cemented gangue backfill body in acid mine water

IF 3.7 2区 材料科学 Q1 METALLURGY & METALLURGICAL ENGINEERING Journal of Central South University Pub Date : 2024-06-24 DOI:10.1007/s11771-024-5650-3
Yong-hui Zhao, Yu-xia Guo, Guo-rui Feng
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Abstract

Cemented gangue backfill technology is an important backfill mining method. However, the acid mine water environment could seriously affect the strength of the cemented gangue backfill body (CGBB). In this study, CGBB specimens were placed in different environments (air, water, H2SO4 solution, and H2SO4 solution coupled with load) to test the strength, resistivity, and ultrasonic pulse velocity (UPV) of CGBB at different ages. The acoustic emission (AE) energy of the specimens during loading was monitored, and the microstructure was analyzed by scanning electron microscopy (SEM) and X-ray diffraction (XRD). Test results showed that: 1) The strength of CGBB cured in air and water gradually slowed down with age. The strength of CGBB in the H2SO4 solution was greater than that of CGBB cured in air or water in the first 90 d. The strength of CGBB under the coupling of the H2SO4 solution and load decreased more slowly with age than that of the single H2SO4 solution; 2) The resistivity and UPV had a good corresponding relationship with the strength of the CGBB. The failure modes of the CGBB after erosion were various, and the CGBB showed different AE energy characteristics at different stages of loading. The surge of AE energy could be used as a precursor to the failure of CGBB; 3) Erosion products compacted CGBB in the early stages and improved its strength. In the later stage, the CGBB cracked under the action of expansion stress and the strength decreased. Applying a 40% stress-to-strength ratio would resist the erosion of the H2SO4 solution. The research could provide a reference for the design of the corrosion resistance of CGBB.

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酸性矿井水中胶结煤矸石回填体的强度演变和劣化规律
胶结矸石回填技术是一种重要的回填采矿方法。然而,酸性矿井水环境会严重影响水泥煤矸石回填体(CGBB)的强度。本研究将 CGBB 试样置于不同的环境(空气、水、H2SO4 溶液和加载 H2SO4 溶液)中,以测试不同龄期 CGBB 的强度、电阻率和超声波脉冲速度(UPV)。监测了加载过程中试样的声发射(AE)能量,并通过扫描电子显微镜(SEM)和 X 射线衍射(XRD)分析了微观结构。测试结果表明1)在空气和水中固化的 CGBB 的强度随着龄期的增加而逐渐降低。在 H2SO4 溶液中固化的 CGBB 在最初 90 d 的强度大于在空气或水中固化的 CGBB,而在 H2SO4 溶液和负载耦合下固化的 CGBB 的强度随龄期的降低速度比单一 H2SO4 溶液固化的 CGBB 慢;2)电阻率和 UPV 与 CGBB 的强度具有良好的对应关系。侵蚀后 CGBB 的失效模式多种多样,在加载的不同阶段,CGBB 表现出不同的 AE 能量特征。AE 能量的激增可作为 CGBB 失效的前兆;3)侵蚀产物在早期阶段压实了 CGBB,提高了其强度。后期,CGBB 在膨胀应力的作用下开裂,强度下降。采用 40% 的应力强度比可以抵抗 H2SO4 溶液的侵蚀。这项研究可为 CGBB 的耐腐蚀性设计提供参考。
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来源期刊
Journal of Central South University
Journal of Central South University METALLURGY & METALLURGICAL ENGINEERING-
CiteScore
6.10
自引率
6.80%
发文量
242
审稿时长
2-4 weeks
期刊介绍: Focuses on the latest research achievements in mining and metallurgy Coverage spans across materials science and engineering, metallurgical science and engineering, mineral processing, geology and mining, chemical engineering, and mechanical, electronic and information engineering
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