Application of fourier transform infrared (FTIR) spectroscopy in sample preparation: Material characterization and mechanism investigation

IF 5.2 Q1 CHEMISTRY, ANALYTICAL Advances in Sample Preparation Pub Date : 2024-06-28 DOI:10.1016/j.sampre.2024.100122
Yahui Gong, Xuerong Chen, Wei Wu
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Abstract

The principle of Fourier Transform Infrared (FTIR) spectroscopy is based on atoms vibration and rotation, and it has become a universal and widely used spectral methodology to detect the internal molecular structures in all kinds of fields. Numerous review articles related to the applications of FTIR spectroscopy have been published in recent years. In addition, more and more scientists are aware the significance role of sample preparation to improve our life quality in life science. However, the application of FTIR spectroscopy in sample preparation hasn't been summarized. Thus, in the current paper, the application of FTIR spectroscopy in sample preparation was reviewed with the focuses on characterization of separation materials including both solid sorbents and liquid extractants, and the extraction mechanisms involved in the separation towards different targets including inorganic molecules such as rare earth elements, organic molecules such as phenolics, pharmaceuticals and illicit-drugs, and biomacromolecules of DNA and proteins. We believe that the current paper will be interested for the researchers in food science, forensic medicine, clinical medicine, environmental analysis and analytical chemistry.

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傅立叶变换红外光谱在样品制备中的应用:材料表征和机理研究
傅立叶变换红外光谱(FTIR)的原理是基于原子的振动和旋转,它已成为在各种领域检测分子内部结构的一种通用而广泛应用的光谱方法。近年来,有关傅立叶变换红外光谱应用的综述文章层出不穷。此外,在生命科学领域,越来越多的科学家意识到样品制备对提高生活质量的重要作用。然而,傅立叶变换红外光谱技术在样品制备中的应用尚未得到总结。因此,本文对傅立叶变换红外光谱在样品制备中的应用进行了综述,重点关注分离材料(包括固体吸附剂和液体萃取剂)的表征,以及针对不同目标物(包括稀土元素等无机分子、酚类等有机分子、药物和违禁药物,以及 DNA 和蛋白质等生物大分子)的分离萃取机制。我们相信,食品科学、法医学、临床医学、环境分析和分析化学领域的研究人员会对本论文感兴趣。
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