Shrinkage and deformation of material extrusion 3D printed parts during sintering: Numerical simulation and experimental validation

IF 8.3 1区 材料科学 Q1 MATERIALS SCIENCE, MULTIDISCIPLINARY Acta Materialia Pub Date : 2024-10-28 DOI:10.1016/j.actamat.2024.120518
Sri Bharani Ghantasala , Gurminder Singh , Jean-Michel Missiaen , Didier Bouvard
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Abstract

Material extrusion 3D printing (ME3DP) combined with sintering is a low-cost additive manufacturing technique for fabricating components of difficult-to-print metals, such as copper, aluminum, and ceramics. However, the sintering process includes complex material science, such as volumetric shrinkage and free structural bending, to identify the relative density and deformation of a 3D printed sample. The prediction of the relative density and deformations during the sintering process provides information to the design engineer to optimize the design of the CAD model before sintering. In this study, a phenomenological model based on constitutive equations was developed to predict the density and structural deformation during the sintering process of pure copper components fabricated by ME3DP using metal injection molding feedstock. The densification rate was determined using shrinkage estimation with an isothermal stairway heating cycle in a vertical dilatometer. Furthermore, different sets of experiments were performed with a load on the probe with long isothermal heating cycles at 850, 900, 950, 1000, and 1050 °C in a vertical dilatometer to estimate the axial viscosity of the copper. The constitutive equations were solved using the solid mechanics module with user-defined creep in COMSOL Multiphysics by considering isotropic assumptions. Two types of geometries, cube and overhanging I section, were used to predict shrinkage and deformation during the sintering process. The developed model successfully predicted the relative density based on shrinkage and structural deformation owing to gravity during the sintering process.

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材料挤压 3D 打印部件在烧结过程中的收缩和变形:数值模拟和实验验证
材料挤压三维打印(ME3DP)与烧结相结合是一种低成本的增材制造技术,可用于制造铜、铝和陶瓷等难以打印的金属部件。然而,烧结过程包括复杂的材料科学,如体积收缩和自由结构弯曲,以确定 3D 打印样品的相对密度和变形。预测烧结过程中的相对密度和变形为设计工程师在烧结前优化 CAD 模型设计提供了信息。本研究建立了一个基于构成方程的现象学模型,用于预测使用金属注射成型原料通过 ME3DP 制造的纯铜部件在烧结过程中的密度和结构变形。通过在垂直扩张仪中进行等温阶梯加热循环,利用收缩率估算确定了致密化率。此外,为了估算铜的轴向粘度,还在垂直扩张仪中以 850、900、950、1000 和 1050°C 的长等温加热循环对探针进行了不同的负载实验。考虑到各向同性假设,使用 COMSOL Multiphysics 中带有用户定义蠕变的固体力学模块求解了构成方程。在预测烧结过程中的收缩和变形时,使用了立方体和悬挂 I 截面两种几何形状。根据烧结过程中的收缩和重力导致的结构变形,所开发的模型成功预测了相对密度。
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来源期刊
Acta Materialia
Acta Materialia 工程技术-材料科学:综合
CiteScore
16.10
自引率
8.50%
发文量
801
审稿时长
53 days
期刊介绍: Acta Materialia serves as a platform for publishing full-length, original papers and commissioned overviews that contribute to a profound understanding of the correlation between the processing, structure, and properties of inorganic materials. The journal seeks papers with high impact potential or those that significantly propel the field forward. The scope includes the atomic and molecular arrangements, chemical and electronic structures, and microstructure of materials, focusing on their mechanical or functional behavior across all length scales, including nanostructures.
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