[The Ascorbic Acid Reference Standard (Control 931) of the National Institute of Health Sciences].

A Kitajima, K Yoshii, H Komatsu, S Ishimitsu, S Okada
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Abstract

Raw ascorbic acid material was tested for preparation of the "Ascorbic Acid Reference Standard (Control 931)". Analytical data obtained were as follows: infrared spectrum, the same as that of the JP Ascorbic Acid Reference Standard; optical rotation -alpha-20D, + 21.4 degrees; melting point, 190.3 degrees C (decomposition); loss on drying, 0.02%; assay result, 100.1% by iodometry. Based on the above findings, the raw material was authorized as the JP Ascorbic Acid Reference Standard (Control 931).

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[国家卫生科学研究所抗坏血酸参考标准(Control 931)]。
为制备“抗坏血酸标准品(对照品931)”,对抗坏血酸原料进行了检测。获得的分析数据如下:红外光谱,与JP抗坏血酸标准品相同;旋光度- α - 20d, + 21.4度;熔点:190.3℃(分解);干燥损失0.02%;碘量法测定结果:100.1%。基于上述发现,该原料被批准为JP抗坏血酸参考标准品(Control 931)。
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