Roughness and Microhardness of Composites after Different Bleaching Techniques

Andreia Leal, A. Paula, A. Ramalho, M. Esteves, M. Ferreira, E. Carrilho
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引用次数: 12

Abstract

Background The aim of this study was to evaluate the roughness and microhardness of SonicFill™ (Kerr), and compare it with Filtek™ Supreme XTE (3M ESPE) after 2 bleaching regimens. Methods Sixty cylindrical specimens (10 × 2 mm) of each of the 2 composites were prepared and divided into 6 groups (n = 20): groups 1, 2: no treatment; groups 3, 4: 10% carbamide peroxide (CP); and groups 5, 6: 35% hydrogen peroxide (HP) plus LED. After treatments, specimens were thermocycled (500 cycles, 5°C/55°C, dwell time 30 minutes). A mechanical roughness tester was employed to measure the surface roughness parameters and the Vickers test to measure microhardness. One-way ANOVA, Tukey and Bonferroni methods with a significance level of 5% were used for the statistical analysis. Results For SonicFill™, there was no statistically significant difference in microhardness between the control group (no. 1) and the bleached groups (nos. 3, 5), but there was difference between CP and HP treatments; for Filtek™ Supreme XTE, there was no significant difference in microhardness among all groups. There was no significant difference in average roughness (Ra) and the root mean square of the roughness (Rq) among all groups. The mean roughness depth (Rz) parameter showed no statistically significant differences among all groups for SonicFill™, but in Filtek™ Supreme XTE, there was a significant increase between control and bleaching treatments; roughness skewness (Rsk) showed no statistically significant differences among all groups for SonicFill™ and Filtek™ Supreme XTE, except for nos. 2 and 4, where the Rsk increased with CP. Conclusions The microhardness of Filtek™ Supreme XTE is less affected by bleaching than that of SonicFill™. Both bleaching treatments affect Rz in Filtek™ Supreme XTE in contrast to SonicFill™, but only the CP treatment affects the Rsk of Filtek™ Supreme XTE, with no significant effect of SonicFill™.
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不同漂白工艺后复合材料的粗糙度和显微硬度
本研究的目的是评估SonicFill™(Kerr)的粗糙度和显微硬度,并将其与Filtek™Supreme XTE (3M ESPE)在两种漂白方案后进行比较。方法制备两种复合材料各60个圆柱形试样(10 × 2 mm),分为6组(n = 20): 1组、2组:不处理;第3,4组:10%过氧化脲(CP);第5,6组:35%过氧化氢(HP)加LED。处理后,试样进行热循环(500次,5°C/55°C,停留时间30分钟)。采用机械粗糙度仪测量表面粗糙度参数,采用维氏试验测量显微硬度。采用单因素方差分析,Tukey和Bonferroni方法,显著性水平为5%。结果SonicFill™的显微硬度与对照组比较差异无统计学意义(p < 0.05)。1)和漂白组(第3、5号),但CP和HP处理之间存在差异;对于Filtek™Supreme XTE,各组之间的显微硬度无显著差异。各组平均粗糙度(Ra)和粗糙度均方根(Rq)差异无统计学意义。SonicFill™的平均粗糙度(Rz)参数在所有组之间没有统计学差异,但在Filtek™Supreme XTE中,对照组和漂白处理之间有显著增加;粗糙度偏度(Rsk)在SonicFill™和Filtek™Supreme XTE各组间差异无统计学意义,但2号和4号组的Rsk随CP增加而增加。结论漂白对Filtek™Supreme XTE显微硬度的影响小于SonicFill™。与SonicFill™相比,两种漂白处理都会影响Filtek™Supreme XTE的Rz,但只有CP处理会影响Filtek™Supreme XTE的Rz,而SonicFill™没有显著影响。
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来源期刊
Journal of Applied Biomaterials & Biomechanics
Journal of Applied Biomaterials & Biomechanics 生物-材料科学:生物材料
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审稿时长
12 months
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