Preparation and Charactrisation of 1,3-dipolar cycloaddition of nitrones with 4-amino antipyrene

D. Mutlaq, Raad J. Ali
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Abstract

Some nitrones (1-5), derived from N–phenyl hydroxylamine with substituted benzaldehyde such as (3-chlorobenzaldehyde, 4-chlorobenzaldehyde, 3-nitrobenzaldehyde, 4-florobenzaldehyde, 2-nitrobenzaldehyde). In subsequent 1,3-dipolar cycloaddition reactions of nitrones with 4-amino antipyrene give isoxazolidines (6-10), They have been identified by 1HNMR, 13CNMR, IR and Mass spectra
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1,3-偶极环加成硝基与4-氨基安替芘的制备与表征
一些氮酮(1-5),由n -苯基羟胺与取代苯甲醛如(3-氯苯甲醛、4-氯苯甲醛、3-硝基苯甲醛、4-氟苯甲醛、2-硝基苯甲醛)衍生而成。硝基酮与4-氨基安替芘的1,3-偶极环加成反应得到异恶唑烷(6-10),并通过1HNMR、13CNMR、IR和质谱对其进行了鉴定
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