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Green synthesis of 3,4-disubstituted isoxazol-5(4H)-one using Gluconic acid aqueous solution as an efficient recyclable medium. 以葡萄糖酸水溶液为高效可回收介质绿色合成3,4-二取代异恶唑-5(4H)- 1。
IF 1.7 Q3 CHEMISTRY, ORGANIC Pub Date : 2023-06-27 DOI: 10.25135/acg.oc.151.2304.2762
Ramesh S. Ghogare, G. Shitre, Anisha R. Patel
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引用次数: 0
Efficient and regioselective acetylation of benzene derivatives with Ac2O in the presence of mercurytetrathiocyanatocobaltate (II) 苯衍生物在三硫代氰基钴酸汞存在下与Ac2O的高效和区域选择性乙酰化反应(II)
IF 1.7 Q3 CHEMISTRY, ORGANIC Pub Date : 2023-06-27 DOI: 10.25135/acg.oc.153.2304.2760
A. Nasreen
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引用次数: 0
Methoxyphenanthrenes: synthesis and structure analysis 甲氧基菲的合成与结构分析
IF 1.7 Q3 CHEMISTRY, ORGANIC Pub Date : 2023-06-27 DOI: 10.25135/acg.oc.152.2305.2795
O. Çakmak, S. Duman, Kıymet Berkil Akar
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引用次数: 0
Synthesis and biological studies of novel hydroxyacetophenone-tetrazole hybrids 新型羟基苯乙酮-四唑杂合体的合成及生物学研究
IF 1.7 Q3 CHEMISTRY, ORGANIC Pub Date : 2023-06-27 DOI: 10.25135/acg.oc.148.2302.2696
G. Dilek, A. Dişli, Esin Eylem Yucesoy, A. Ozturk
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引用次数: 0
Synthesis of heterocyclic compounds from camphor 以樟脑为原料合成杂环化合物
IF 1.7 Q3 CHEMISTRY, ORGANIC Pub Date : 2023-05-22 DOI: 10.25135/acg.oc.150.2303.2741
E. Alwan, Marwa Bayoumy, R. Mohareb
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引用次数: 0
An efficient zinc acetate dihydrate-catalyzed green protocol for the synthesis of 2,3-dihydroquinazolin-4(1H)-ones 高效二水乙酸锌催化合成2,3-二氢喹唑啉-4(1H)-酮的绿色方案
IF 1.7 Q3 CHEMISTRY, ORGANIC Pub Date : 2023-05-11 DOI: 10.25135/acg.oc.149.2303.2742
B. Chinta, Satyadev N.V.S.S. Turlapati, Venkata Adilakshmi Gaddaguti
: By condensation from substituted carbonyl compounds and anthranilamide under toluene reflux conditions, a wide range of 2,3-dihydroquinazolin-4(1 H )-ones were produced in fair to good yields with the use of a Lewis acid catalyst Zn(OAc) 2 •2H 2 O (10 mol%), which is inexpensive, accessible, and environmentally friendly. All the synthesized compounds were properly described using melting point, IR, NMR, and mass spectral studies, and the findings were compared with information from the earlier literature. The new method has a number of advantages over the traditional methods for the synthesis of divergent 2,3-dihydroquinazolin-4(1 H )-ones, including a higher product conversion, a wide substrate range, and the absence of undesirable side products. Aliphatic, heteroaromatic and aromatic carbonyl compounds were well tolerated under the optimized reaction conditions.
:通过在甲苯回流条件下由取代羰基化合物和邻氨基苯甲酰胺缩合,使用廉价、可获得且环境友好的路易斯酸催化剂Zn(OAc)2•2H2O(10mol%),以相当好的产率生产了广泛的2,3-二氢喹唑啉-4(1H)-酮。使用熔点、IR、NMR和质谱研究对所有合成的化合物进行了适当的描述,并将这些发现与早期文献中的信息进行了比较。与传统方法相比,新方法在合成不同的2,3-二氢喹唑啉-4(1H)-酮方面具有许多优点,包括较高的产物转化率、较宽的底物范围和不存在不良副产物。在优化的反应条件下,脂肪族、杂芳香族和芳香羰基化合物具有良好的耐受性。
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引用次数: 0
Synthesis and biological activities of substituted 1,3,4-oxadiazolines 取代1,3,4-恶二唑啉的合成及其生物活性
IF 1.7 Q3 CHEMISTRY, ORGANIC Pub Date : 2023-03-30 DOI: 10.25135/acg.oc.146.2302.2717
Hany M. M. Dalloul, Kholoud R. Abu Yunis
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引用次数: 0
Synthesis and structure analysis of methyl 1-benzyl-5-(phenylamino)methyl)-1H-1,2,3-triazole-4-carboxylate 1-苄基-5-(苯基氨基)甲基)-1H-1,2,3-三唑-4-羧酸甲酯的合成与结构分析
IF 1.7 Q3 CHEMISTRY, ORGANIC Pub Date : 2023-03-28 DOI: 10.25135/acg.oc.147.2302.2631
A. Altundas, Güler Yagiz Erdemir
{"title":"Synthesis and structure analysis of methyl 1-benzyl-5-(phenylamino)methyl)-1H-1,2,3-triazole-4-carboxylate","authors":"A. Altundas, Güler Yagiz Erdemir","doi":"10.25135/acg.oc.147.2302.2631","DOIUrl":"https://doi.org/10.25135/acg.oc.147.2302.2631","url":null,"abstract":"","PeriodicalId":19553,"journal":{"name":"Organic Communications","volume":" ","pages":""},"PeriodicalIF":1.7,"publicationDate":"2023-03-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"43644231","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis and biological evaluation of new 4-thiazolidinone derivatives of flurbiprofen 新型氟比洛芬4-噻唑烷酮衍生物的合成及生物学评价
IF 1.7 Q3 CHEMISTRY, ORGANIC Pub Date : 2023-03-13 DOI: 10.25135/acg.oc.144.2212.2653
Sevil Şenkardeş, P. Süzgün, Merve Gürboğa, Özlem BİNGÖL ÖZAKPINAR, Ş. Küçükgüzel
{"title":"Synthesis and biological evaluation of new 4-thiazolidinone derivatives of flurbiprofen","authors":"Sevil Şenkardeş, P. Süzgün, Merve Gürboğa, Özlem BİNGÖL ÖZAKPINAR, Ş. Küçükgüzel","doi":"10.25135/acg.oc.144.2212.2653","DOIUrl":"https://doi.org/10.25135/acg.oc.144.2212.2653","url":null,"abstract":"","PeriodicalId":19553,"journal":{"name":"Organic Communications","volume":" ","pages":""},"PeriodicalIF":1.7,"publicationDate":"2023-03-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"48619743","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis of some piperazine/piperidine amides of chromone-2-carboxylic acid as potential soluble epoxide hydrolase (sEH) inhibitors 作为可溶性环氧化物水解酶(sEH)抑制剂的一些哌嗪类/哌啶类铬-2-羧酸酰胺的合成
IF 1.7 Q3 CHEMISTRY, ORGANIC Pub Date : 2023-03-10 DOI: 10.25135/acg.oc.145.2302.2705
Tugçe Gur Maz, H. B. Caliskan
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引用次数: 0
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Organic Communications
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