[测量工作区空气中茜素浓度的光度法和色谱法]。

E G Ivaniuk, Iu A Kolievskaia, N E Pisareva, S V Mikhaĭlik, I D Perets
{"title":"[测量工作区空气中茜素浓度的光度法和色谱法]。","authors":"E G Ivaniuk,&nbsp;Iu A Kolievskaia,&nbsp;N E Pisareva,&nbsp;S V Mikhaĭlik,&nbsp;I D Perets","doi":"","DOIUrl":null,"url":null,"abstract":"<p><p>Two methods were applied to evaluation of acelysine level. Spectrophotometric one was based on reaction with p-nitrophenyldiasonium and evaluation of the product optic density at 510 nm. The second was chromatography in thin layer, where a mixture of n-butanol, formic acid and water was used as an eluent and 0.2% ninhydrin solution in butanol and 3 ml of ice acetic acid (60-70 degrees C) served as a developer. Both methods are supposed to evaluate acelysine level in the air of working area, when a half of MAC and admixtures are present.</p>","PeriodicalId":12679,"journal":{"name":"Gigiena truda i professional'nye zabolevaniia","volume":" 11-12","pages":"35-7"},"PeriodicalIF":0.0000,"publicationDate":"1992-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"[Photometric and chromatographic methods of measuring the concentration of acelysin in the air of a work area].\",\"authors\":\"E G Ivaniuk,&nbsp;Iu A Kolievskaia,&nbsp;N E Pisareva,&nbsp;S V Mikhaĭlik,&nbsp;I D Perets\",\"doi\":\"\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p><p>Two methods were applied to evaluation of acelysine level. Spectrophotometric one was based on reaction with p-nitrophenyldiasonium and evaluation of the product optic density at 510 nm. The second was chromatography in thin layer, where a mixture of n-butanol, formic acid and water was used as an eluent and 0.2% ninhydrin solution in butanol and 3 ml of ice acetic acid (60-70 degrees C) served as a developer. Both methods are supposed to evaluate acelysine level in the air of working area, when a half of MAC and admixtures are present.</p>\",\"PeriodicalId\":12679,\"journal\":{\"name\":\"Gigiena truda i professional'nye zabolevaniia\",\"volume\":\" 11-12\",\"pages\":\"35-7\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1992-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Gigiena truda i professional'nye zabolevaniia\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Gigiena truda i professional'nye zabolevaniia","FirstCategoryId":"1085","ListUrlMain":"","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

采用两种方法评价乙酰赖氨酸水平。分光光度法与对硝基苯二钠反应,测定产物在510 nm处的光密度。二是薄层色谱法,以正丁醇、甲酸和水的混合物为洗脱液,以0.2%丁醇溶液和3ml冰醋酸(60-70℃)为显像剂。两种方法都适用于在半MAC和外加剂存在的情况下,对工作区域空气中乙酰赖氨酸水平的评价。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
[Photometric and chromatographic methods of measuring the concentration of acelysin in the air of a work area].

Two methods were applied to evaluation of acelysine level. Spectrophotometric one was based on reaction with p-nitrophenyldiasonium and evaluation of the product optic density at 510 nm. The second was chromatography in thin layer, where a mixture of n-butanol, formic acid and water was used as an eluent and 0.2% ninhydrin solution in butanol and 3 ml of ice acetic acid (60-70 degrees C) served as a developer. Both methods are supposed to evaluate acelysine level in the air of working area, when a half of MAC and admixtures are present.

求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
期刊最新文献
[Characteristics of modification of lipids of erythrocyte membranes and blood plasma in combined action of pesticides after physical exercise of varied intensity]. [Changes in the serological indices of the immune status of workers in contact with raw foodstuffs contaminated by mycotoxins]. [A method for isolating a complex epoxide-containing antigen and its use for the diagnosis of allergic diseases]. [The comparative characteristics of the cytochemical indices of the peripheral blood neutrophils in the separate administration of organochlorine and organophosphate pesticides against a background of dynamic loading with different intensities]. [The immunostimulating properties of erythrocytes subjected to the action of ultraviolet irradiation and electromagnetic radiation during vibration exposure].
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1