R. Irwanto, A. Kasim, Sahadi Didi Ismanto
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摘要

精油是一种具有植物特有气味且易挥发的精油。精油可以通过几种方法获得,如蒸馏、膨化、浸渍和提取。蒸馏是一种根据沸点差异分离所需化合物(精油)的技术。细化过程以几种方式进行,包括以枯萎、干燥和缩小尺寸的形式进行预处理。蒸馏也可以通过不同的蒸馏时间来完成。蒸馏过程分为肉桂叶的制备、肉桂叶的制备、肉桂叶的中试蒸馏、肉桂叶精油与蒸馏水的分离、肉桂叶精油蒸馏后的理化性质分析等阶段。本研究采用因子完全随机设计(CRD),不同的蒸馏时间(3小时、4小时、5小时、6小时和7小时)和叶片条件(新鲜和干燥叶片条件)进行2次重复。数据分析采用5%显著性水平的F检验,如果结果有显著性差异,则继续采用“Duncan’s New Multiple Range test”(DNMRT)检验。结果表明,鲜叶和干叶的最佳蒸馏时间为5 h,产率为0.39%,比重为1.0015,折射率为1.526,旋光度为-4.640,肉桂醛含量为14.21%。
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Penentuan Kadar Minyak Atsiri Daun Kayu Manis (Cinnamomum burmannii, Blume) dengan Perlakuan Pendahuluan pada Daun
Essential oils are essential oils that have a characteristic smell of plants and are volatile. Essential oils can be obtained by several processes such as distillation, enfleuration, maceration and extraction. Distillation is a technique used to separate the desired compound (essential oil) based on differences in boiling points. The detailing process is carried out in several ways including pre-treatment in the form of withering, drying and size reduction. Distillation can also be done by giving different distillation times. The distillation process was carried out through the stages of preparation of cinnamon leaves for determination of essential oil content, preparation of cinnamon leaves for pilot-scale distillation, separation of cinnamon leaf essential oil with distilled water, as well as analysis of the physical and chemical properties of distilled cinnamon leaf essential oil. This study used a Factorial Completely Randomized Design (CRD) with differences in distillation time (3 hours, 4 hours, 5 hours, 6 hours, and 7 hours), and leaf conditions (fresh and dry leaf conditions) for 2 replications. Data analysis was carried out with the F test at a 5% significance level, if the results were significantly different then the analysis continued with the "Duncan's New Multiple Range Test" (DNMRT) test. The results showed that the optimum distillation time was 5 hours for fresh and dry leaves with chemical and physical properties, namely yield of 0.39%, specific gravity of 1.0015, refractive index of 1.526, optical rotation -4.640 and cinnamaldehyde content of 14.21%.
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