血浆中吡罗昔康的密度测定。

Ceskoslovenska farmacie Pub Date : 1991-03-01
M Peterková, O Matousová, V Rejholec
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引用次数: 0

摘要

用氯仿-无水乙醇-苯-水氨(20:15:15:5 .5)体系从酸性介质中提取吡罗昔康,在硅胶薄层上进行分离。采用密度法(Hg灯,滤光片FL - 39, 330 nm)测定染色液的荧光强度。本法的检出限为0.020微克/毫升血浆。
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[Densitometric determination of piroxicam in plasma].

Piroxicam was extracted from acid medium into chloroform and isolated on a thin layer of silica gel with the use of the system chloroform - absolute ethanol - benzene - aqueous ammonia (20:15:15:0.5). The intensity of fluorescence of stains was measured densitometrically (an Hg lamp, a filter FL - 39, 330 nm). The limit of detection of the stain is 0.020 microgram/ml of plasma.

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