E. Podda, Eleanor Dodd, M. Arca, M. Aragoni, Vito Lippolis, S. Coles, Anna Pintus
{"title":"产品名称","authors":"E. Podda, Eleanor Dodd, M. Arca, M. Aragoni, Vito Lippolis, S. Coles, Anna Pintus","doi":"10.3390/m1753","DOIUrl":null,"url":null,"abstract":"N,N′-Dipropyloxamide (1) was synthesised by the reaction between diethyloxalate and n-propylamine in ethanol. Compound 1 was fully characterised by both microanalytical (elemental analysis, melting point determination) and spectroscopic means (FT-IR and NMR spectroscopy). Crystals suitable for single crystal X-ray diffraction were isolated by the slow evaporation of a methyl alcohol solution of the compound. The resulting crystal structure shows the prominent role exerted by intermolecular hydrogen bonds in the crystal packing.","PeriodicalId":18761,"journal":{"name":"Molbank","volume":"37 3","pages":""},"PeriodicalIF":0.6000,"publicationDate":"2023-12-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"N,N′-Dipropyloxamide\",\"authors\":\"E. Podda, Eleanor Dodd, M. Arca, M. Aragoni, Vito Lippolis, S. Coles, Anna Pintus\",\"doi\":\"10.3390/m1753\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"N,N′-Dipropyloxamide (1) was synthesised by the reaction between diethyloxalate and n-propylamine in ethanol. Compound 1 was fully characterised by both microanalytical (elemental analysis, melting point determination) and spectroscopic means (FT-IR and NMR spectroscopy). Crystals suitable for single crystal X-ray diffraction were isolated by the slow evaporation of a methyl alcohol solution of the compound. The resulting crystal structure shows the prominent role exerted by intermolecular hydrogen bonds in the crystal packing.\",\"PeriodicalId\":18761,\"journal\":{\"name\":\"Molbank\",\"volume\":\"37 3\",\"pages\":\"\"},\"PeriodicalIF\":0.6000,\"publicationDate\":\"2023-12-22\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Molbank\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.3390/m1753\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"CHEMISTRY, ORGANIC\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Molbank","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.3390/m1753","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"CHEMISTRY, ORGANIC","Score":null,"Total":0}
引用次数: 0
摘要
N,N′-Dipropyloxamide (1) 是通过二乙氧基丙酸盐和正丙胺在乙醇中的反应合成的。通过微量分析（元素分析、熔点测定）和光谱分析（傅立叶变换红外光谱和核磁共振光谱）对化合物 1 进行了全面鉴定。通过缓慢蒸发化合物的甲醇溶液，分离出了适合进行单晶 X 射线衍射的晶体。由此得到的晶体结构表明，分子间氢键在晶体堆积中发挥了重要作用。
N,N′-Dipropyloxamide (1) was synthesised by the reaction between diethyloxalate and n-propylamine in ethanol. Compound 1 was fully characterised by both microanalytical (elemental analysis, melting point determination) and spectroscopic means (FT-IR and NMR spectroscopy). Crystals suitable for single crystal X-ray diffraction were isolated by the slow evaporation of a methyl alcohol solution of the compound. The resulting crystal structure shows the prominent role exerted by intermolecular hydrogen bonds in the crystal packing.
京公网安备 11010802042870号
京ICP备2023020795号-1
分享
求助内容：
应助结果提醒方式：
扫码关注我们
