基于英华尔的双法布里-珀罗腔折射仪,用于评估压力,压力不确定度在亚兆帕(mPa)以下区域

I. Silander, J. Zakrisson, M. Zelan, O. Axner
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摘要

采用气体调制方法的英发双法布里-珀罗腔折射仪的更新版,在低压状态下评估气体压力的能力得到了鉴定,低压状态是指仪器主要受限于不确定度表达式[(a)2+(b×P)2]1/2 中常数 a 的状态。我们首先得出结论,这种能力主要受到三个实体的限制,即空腔重复性、抽空(测量)腔中的残余气体压力以及测量腔中的气体污染(源于泄漏和放气)。然后,我们提出并利用各种方法,分别从这些实体中估算出更新折射仪的不确定性。我们发现,在使用 100 秒的气体调制周期和氮气时,系统可以评估低压状态下的压力,扩展不确定度 (k=2) 为 0.75 mPa,主要受限于空腔重复性和氢气放气。这比之前评估的仪器低压性能低 1 个数量级以上。
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An Invar-based dual Fabry–Perot cavity refractometer for assessment of pressure with a pressure independent uncertainty in the sub-mPa region
An updated version of an Invar-based dual Fabry–Perot cavity refractometer utilizing the gas modulation methodology has been characterized with regard to its ability to assess gas pressure in the low pressure regime, defined as the regime in which the instrumentation is mainly limited by the constant term a in the [(a)2+(b×P)2]1/2 expression for the uncertainty. It is first concluded that this ability is predominantly limited by three entities, viz., the empty cavity repeatability, the residual gas pressures in the evacuated (measurement) cavity, and the contamination of the gas residing in the measurement cavity that originates from leaks and outgassing. We then present and utilize methods to separately estimate the uncertainty of the updated refractometer from these entities. It was found that, when utilizing gas modulation cycles of 100 s and when addressing nitrogen, the system can assess pressure in the low pressure regime with an expanded uncertainty (k=2) of 0.75 mPa, mainly limited by the empty cavity repeatability and outgassing of hydrogen. This is more than 1 order of magnitude below the previously assessed low pressure performance of the instrumentation.
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