通过碱性处理和纳米粘土加固协同增强环氧基椰壳纤维复合材料的力学性能

Puneethraj Hebbalu Puttaswamygowda, Sathyashankara Sharma, Achutha Kini Ullal, Manjunath Shettar
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摘要

本研究探讨了在环氧树脂复合材料中加入椰壳纤维和纳米粘土的协同效应。椰壳纤维是一种可再生且具有成本效益的天然纤维,经过碱性处理后可影响其与环氧树脂基体形成强界面结合的能力。为了进一步提高复合材料的机械性能,还引入了用氨基丙基三乙氧基硅烷和十八烷基胺进行表面改性的蒙脱石纳米土。研究调查了环氧树脂中椰壳纤维含量(20、30 和 40 wt%)和纳米粘土含量(0、2 和 4 wt%)的不同组合。复合材料是通过开放成型工艺制成的,其机械性能分别根据 ASTM D638 和 D7264 标准通过拉伸和弯曲测试进行评估。结果发现,40 wt%粗纤维增强环氧树脂复合材料的拉伸强度和弯曲强度分别为 77.99 兆帕和 136.13 兆帕,比纯环氧树脂分别高出 44% 和 23%。此外,在添加了 4 wt%的纳米粘土作为额外增强材料后,拉伸强度提高了 23%,弯曲强度提高了 31.4%。采用扫描电子显微镜对拉伸试验中断裂的试样进行断口分析。这项研究强调了了解天然纤维、纳米粘土和环氧树脂之间的相互作用对于优化复合材料在实际应用中的性能的重要性。
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Synergistic Enhancement of the Mechanical Properties of Epoxy-Based Coir Fiber Composites through Alkaline Treatment and Nanoclay Reinforcement
This study explores the synergistic effects of incorporating coir fibers and nanoclay into epoxy resin composites. Coir, a renewable and cost-effective natural fiber, undergoes an alkaline treatment to influence its ability to form strong interfacial bonding with the epoxy matrix. To further enhance the mechanical properties of the composite, montmorillonite nanoclay, surface-modified with aminopropyltriethoxysilane and octadecyl amine, is introduced. The research investigates different combinations of coir fiber content (20, 30, and 40 wt%) and nanoclay loading (0, 2, and 4 wt%) with epoxy resin. The composites are fabricated through an open molding process, and the mechanical properties are evaluated using tensile and flexural tests according to the ASTM D638 and D7264 standards, respectively. The tensile and flexural strengths of the 40 wt% coir fiber-reinforced epoxy composite are found to be 77.99 MPa and 136.13 MPa, which are 44% and 23% greater than pure epoxy, respectively. Furthermore, the strengths displayed a 23% improvement in tensile strength with 4 wt% and a 31.4% improvement in flexural strength with 2 wt% nanoclay as additional reinforcement. Scanning electron microscopy is employed for fractographic analysis of the fractured specimens from the tensile test. The study underscores the importance of understanding the interplay between natural fibers, nanoclay, and epoxy resin for optimizing the composite’s performance in real-world applications.
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