利用新鲜燕麦花提取物合成金纳米粒子的两种合成方法研究

T. Chimsook
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引用次数: 0

摘要

本研究利用蝴蝶豌豆(Clitoria ternatea)的花提取物,通过两种合成方法(包括 1)加热法 2)微波辅助萃取法,研究了 AuNPs 的合成。蝶形花提取物(CT 提取物)采用微波辅助萃取法制备。使用 CT 提取物合成 AuNPs 的最佳条件是微波辅助提取(1,000 瓦,3 分钟)。通过透射电子显微镜(TEM)和 X 射线衍射分析(XRD)分别研究了微波辅助萃取合成的 AuNPs 的形态。合成的 AuNPs 的 TEM 图像也显示大多数纳米粒子呈球形,X 射线衍射图在 2θ = 38.44°、44.41°、65.03° 和 77.58°处分别出现了一个强峰,对应于面心立方结构的 (111)、(200)、(220) 和 (311) 面。
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Study of Two Synthesized Methods of Gold Nanoparticles Synthesis Using Fresh Flowers Extracts of Clitoria ternatea
In this research, the syntheses of AuNPs using the flowers extract of butterfly pea (Clitoria ternatea) were studied by two synthesized methods including 1) heating 2) microwave assisted extraction. C. ternatea extract (CT extract) was prepared using the microwave assisted extraction. The best condition for syntheses of AuNPs using CT extract were performed using microwave assisted extraction (1,000 watt for 3 min). The morphology of the synthesized AuNPs from microwave assisted extraction was investigated by transmission electron microscopy (TEM) and X-Ray diffraction analysis (XRD), respectively. The TEM image of synthesized AuNPs also showed that most nanoparticles were in a spherical shape and XRD pattern presented an intense peak at 2θ = 38.44°, 44.41°, 65.03° and 77.58°, respectively which correspond to face centered cubic structure with (111), (200), (220) and (311) plane.
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