通过 X-CT、MIP 和 SEM 试验表征持续高温条件下碱激活粉煤灰-矿渣混凝土的微观/宏观尺度特性

IF 7.1 3区 材料科学 Q1 GREEN & SUSTAINABLE SCIENCE & TECHNOLOGY Materials Today Sustainability Pub Date : 2024-11-01 DOI:10.1016/j.mtsust.2024.101036
Hongqiang Ma , Congcong Fu , Jialong Wu , Xinhua Yuan , Chao Wu , Jingjing Feng
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引用次数: 0

摘要

基于 X-CT、MIP 和 SEM 测试,研究了碱激活粉煤灰-矿渣(AAFS)混凝土在持续高温下的微观/宏观尺度演变。结果表明,在 60 °C 时,C-S-H 和 C-A-S-H 凝胶相的失水是持续的(约 60d)。根据 X-CT 试验得出的中尺度孔隙体积变化规律与 MIP 试验得出的微尺度孔隙体积变化规律一致。二维分形维数可用于定性评估 AAFS 混凝土在持续高温作用后的内部微裂缝和微结构复杂性。在 100 ℃、150 ℃ 和 200 ℃ 的作用下,质量损失率可在 3d-7d 内达到稳定,且不存在由初始失水引起的微裂缝和孔隙累积效应。在持续高温作用下,AAFS 混凝土的内部孔隙结构、微裂缝和微观结构变化具有持久性,这些持久性变化导致 AAFS 混凝土的力学性能发生显著变化。
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Micro/meso scales characterization of alkali-activated fly ash-slag concrete under sustained high-temperatures with X-CT, MIP, and SEM tests
Based on X-CT, MIP, and SEM tests, the micro/meso scales evolutions of alkali-activated fly ash-slag (AAFS) concrete under sustained high temperatures are studied. The results show that the water loss of the C–S–H and C-A-S-H gel phases at 60 °C is continuous (about 60d). The variation law of meso-scale pore volume based on the X-CT test is consistent with that of micro-scale pore volume obtained by the MIP test. The 2D fractal dimension can be used to qualitatively evaluate the internal micro-cracks and microstructure complexity of AAFS concrete after sustained high-temperature action. The mass loss rate can reach stability within 3d-7d under the action of 100 °C, 150 °C, and 200 °C, and there is no cumulative effect of micro-cracks and pores caused by initial water loss. Under sustained high-temperatures, the internal pore structure, micro-cracks, and microstructure changes of AAFS concrete are persistent, and these persistent changes lead to a significant change in the mechanical properties of AAFS concrete.
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来源期刊
CiteScore
5.80
自引率
6.40%
发文量
174
审稿时长
32 days
期刊介绍: Materials Today Sustainability is a multi-disciplinary journal covering all aspects of sustainability through materials science. With a rapidly increasing population with growing demands, materials science has emerged as a critical discipline toward protecting of the environment and ensuring the long term survival of future generations.
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