筛选分析:一种实时分析和更环保的微波辅助过硫酸盐分解调味饮料的替代方法

IF 4.1 Q1 CHEMISTRY, ANALYTICAL Talanta Open Pub Date : 2023-08-01 DOI:10.1016/j.talo.2023.100229
Rodolfo M.M. Santana , Lidio Pereira Junior , Marcos Diogo S. Pereira , Mauro Korn
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引用次数: 0

摘要

提议的程序旨在在仪器确定元素和实时决策之前生成有关有机物分解效率的信息。在存在有机化合物样品的情况下,辐照时间(至少20秒或更长)始终高于在无有机物溶液中观察到的MnO4 -的辐照时间(10±1秒,n = 6)。此外,在所有与观察到的目标化合物无关的溶液中,RCC值均≤14%。测定过硫酸盐分解前后样品的总碳含量,除葡萄味水(RCC = 85%)外,碳含量降低95%。微波辅助S2O82−/Mn2+系统为饮料矿化提供了一种快速、清洁和轻松的方法,从而节省了材料、能源和时间。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

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Screening analysis: An alternative for real-time analysis and greener microwave-assisted persulfate decomposition of flavored beverages

The proposed procedure aims to generate information about the decomposition efficiency of organic matter before the instrumental determination of elements and real-time decision-making. In the presence of organic compounds samples, the irradiation time was consistently higher (at least 20 s or more) than that observed for the appearance of MnO4 in organic matter-free solutions (10±1 s, n = 6). Moreover, RCC values ≤14% were determined for all solutions independent of the target compound observed. Total carbon was determined in samples before and after persulfate decomposition, with a 95% reduction in the carbon content, except for grape-flavored waters (RCC = 85%). The microwave-assisted S2O82−/Mn2+ system allowed a fast, clean and effortless approach leading to material, energy, and time-saving method for mineralizing beverages.

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来源期刊
Talanta Open
Talanta Open Chemistry-Analytical Chemistry
CiteScore
5.20
自引率
0.00%
发文量
86
审稿时长
49 days
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