{"title":"技术说明:使用FIMS测定污水污泥、沉积物和土壤样品中的汞含量。","authors":"T Guo, J Baasner","doi":"10.1155/S1463924696000272","DOIUrl":null,"url":null,"abstract":"Stock standard mercury solution #1, 1000 mg/1, was prepared from Merk Tritisol(R). Stock mercury solutions #2 and #3:10 mg/1 and mg/1 respectively, were prepared by further dilution of the stock standard solution #1. Calibration standards at different mercury levels were prepared from stock solutions #2 and #3 by further dilution in 3% v/v HC1. Calibration standard solutions used for the measurement of sewage samples were 0\"00, 5\"00, 10\"00, 15-00, 20\"00, and 30\"00 lg/1. Calibration standard solutions used for the measurement of soil and sediment samples were 0\"00, 3-00, 5\"00, 7\"00, and 10\"00 tg/1. According to DIN 38 405-E 12, the standard solutions should contain 1% v/v of the stabilizing solution.","PeriodicalId":22600,"journal":{"name":"The Journal of Automatic Chemistry","volume":"18 6","pages":"221-3"},"PeriodicalIF":0.0000,"publicationDate":"1996-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1155/S1463924696000272","citationCount":"8","resultStr":"{\"title\":\"Technical Note: Using FIMS to determine mercury content in sewage sludge, sediment and soil samples.\",\"authors\":\"T Guo, J Baasner\",\"doi\":\"10.1155/S1463924696000272\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Stock standard mercury solution #1, 1000 mg/1, was prepared from Merk Tritisol(R). Stock mercury solutions #2 and #3:10 mg/1 and mg/1 respectively, were prepared by further dilution of the stock standard solution #1. Calibration standards at different mercury levels were prepared from stock solutions #2 and #3 by further dilution in 3% v/v HC1. Calibration standard solutions used for the measurement of sewage samples were 0\\\"00, 5\\\"00, 10\\\"00, 15-00, 20\\\"00, and 30\\\"00 lg/1. Calibration standard solutions used for the measurement of soil and sediment samples were 0\\\"00, 3-00, 5\\\"00, 7\\\"00, and 10\\\"00 tg/1. According to DIN 38 405-E 12, the standard solutions should contain 1% v/v of the stabilizing solution.\",\"PeriodicalId\":22600,\"journal\":{\"name\":\"The Journal of Automatic Chemistry\",\"volume\":\"18 6\",\"pages\":\"221-3\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1996-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1155/S1463924696000272\",\"citationCount\":\"8\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"The Journal of Automatic Chemistry\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1155/S1463924696000272\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"The Journal of Automatic Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1155/S1463924696000272","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Technical Note: Using FIMS to determine mercury content in sewage sludge, sediment and soil samples.
Stock standard mercury solution #1, 1000 mg/1, was prepared from Merk Tritisol(R). Stock mercury solutions #2 and #3:10 mg/1 and mg/1 respectively, were prepared by further dilution of the stock standard solution #1. Calibration standards at different mercury levels were prepared from stock solutions #2 and #3 by further dilution in 3% v/v HC1. Calibration standard solutions used for the measurement of sewage samples were 0"00, 5"00, 10"00, 15-00, 20"00, and 30"00 lg/1. Calibration standard solutions used for the measurement of soil and sediment samples were 0"00, 3-00, 5"00, 7"00, and 10"00 tg/1. According to DIN 38 405-E 12, the standard solutions should contain 1% v/v of the stabilizing solution.
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