Diogo de Azevedo Miranda, Carlos Eduardo dos Santos Bertoldo, Glaucia Maria Bovi Ambrosano, Flávio Henrique Baggio Aguiar, Débora Alves Nunes Leite Lima, José Roberto Lovadino
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Twice a day, the samples were immersed in 2 ml of the mouthwashes (12 hr intervals). After the 30-day period, the discs were reweighed (m2). The reconditioning in the desiccator was done until a constant mass (m3) was obtained. The data of DC% were analyzed by analysis of variance (ANOVA) in split plots and the results showed statistical difference when photoactivated to 6 mm from the tip of the curing unit. The sorption data were submitted to two-way ANOVA and Tukey's Test at a 5% level of significance and it was observed that a statistical difference (P < 0.05) was only cured when the distance was 6 mm, but there was no difference in sorption between mouthwashes. The solubility data were analyzed by Kruskal-Wallis's Test (P = 0.05) and Dunn's Test, since a non-normal data distribution was observed. 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引用次数: 0
摘要
本体外研究的目的是评估纳米填充复合材料(Filtek™Z350)在三个固化光距离(0 mm, 3 mm和6 mm)下从顶部光激活的吸附(Sp)和溶解度(Sl),并浸泡在三种不同的漱口水中(Plax Fresh Mint, Plax无酒精和Plax美白)。制备了6 mm Ø和1 mm高的样品(n = 5),利用傅里叶变换红外光谱仪获得了圆盘的初始转化率(DC%)。然后,将样品置于37°C的干燥器中并称重,直到获得恒定质量(m1)。将这些光盘浸泡在漱口水中30天。每天两次,将样品浸入2毫升漱口水中(间隔12小时)。30 d后,重新称重(m2)。在干燥器中进行整修,直到获得恒定质量(m3)。对DC%的数据进行方差分析(ANOVA),在离固化装置尖端6 mm处进行光活化,结果有统计学差异。对吸附数据进行双因素方差分析和Tukey’s检验,在5%的显著性水平下,只有当距离为6 mm时才有统计学差异(P < 0.05),但两种漱口水的吸附量没有差异。溶解度数据呈非正态分布,采用Kruskal-Wallis检验(P = 0.05)和Dunn检验进行分析。该值为负,这意味着质量增加,掩盖了实际的溶解度。
Effect of curing light distance and different mouthwashes on the sorption and solubility of a nanofilled composite.
The aim of this in vitro study was to evaluate the sorption (Sp) and solubility (Sl) of a nanofilled composite (Filtek Z350) light-activated from the top in three curing light distances (0 mm, 3 mm and 6 mm) and immersed in three different mouthwashes (Plax Fresh Mint, Plax Alcohol Free, and Plax Whitening). Specimens (6 mm Ø and 1 mm height) were prepared (n = 5) and initially the degree of conversion (DC%) of discs was obtained by using a fourier transform infrared spectrometer. Then, the specimens were placed in a desiccator at 37°C and were weighed until a constant mass (m1) was obtained. The discs were immersed in the mouthwashes for 30 days. Twice a day, the samples were immersed in 2 ml of the mouthwashes (12 hr intervals). After the 30-day period, the discs were reweighed (m2). The reconditioning in the desiccator was done until a constant mass (m3) was obtained. The data of DC% were analyzed by analysis of variance (ANOVA) in split plots and the results showed statistical difference when photoactivated to 6 mm from the tip of the curing unit. The sorption data were submitted to two-way ANOVA and Tukey's Test at a 5% level of significance and it was observed that a statistical difference (P < 0.05) was only cured when the distance was 6 mm, but there was no difference in sorption between mouthwashes. The solubility data were analyzed by Kruskal-Wallis's Test (P = 0.05) and Dunn's Test, since a non-normal data distribution was observed. The values were negative, which means that there was a mass gain, masking the real solubility.