无溶剂绿色高效一锅合成二氢吡喃[3,2-c]铬衍生物。

ISRN Organic Chemistry Pub Date : 2013-10-24 eCollection Date: 2013-01-01 DOI:10.1155/2013/185120
Shubha Jain, Deepika Rajguru, Balwant S Keshwal, Aman D Acharya
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引用次数: 13

摘要

介绍了一种在无溶剂条件下,以DABCO为催化剂,芳香族醛、丙二腈和4-羟基香豆素三组分一锅缩合合成二氢吡喃[3,2-c]铬衍生物的快速、清洁、高效方法。本方法具有反应条件温和、反应时间短、产物分离容易、收率高等优点。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

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Solvent-Free Green and Efficient One-Pot Synthesis of Dihydropyrano[3,2-c]chromene Derivatives.

A rapid, clean, and highly efficient method for synthesis of dihydropyrano[3,2-c]chromene derivatives by one-pot, three-component condensation of aromatic aldehydes, malononitrile, and 4-hydroxycoumarin using DABCO as catalyst in solvent-free neat conditions is described. The present method has the advantages of mild reaction conditions, short reaction times, easy isolation of products, and excellent yields.

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