热液老化后整体氧化锆和堆芯氧化锆的半透明性。

Salma M Fathy, Abeer A El-Fallal, Salwa A El-Negoly, Abu Baker El Bedawy
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引用次数: 45

摘要

目的:评价水热老化对部分稳定的含氧化钇(Y-TZP)单晶氧化锆、全磨氧化锆和芯型氧化锆的透光性的影响。方法:将Y-TZP单片型和芯型材料各20个(1和10 mm)圆盘状试样,按照生产厂家的说明书进行铣削和烧结。根据使用的Y-TZP类型将最终标本分为两组。用漫反射法在白色和黑色背景上测量半透明参数(TP);采用x射线衍射(XRD)和扫描电子显微镜(SEM)对两种Y-TZP合金时效前后的微观结构进行了分析。TP值数据采用Student’st检验进行统计学分析。结果:整体Y-TZP老化前TP均值最高(16.4±0.316),而核心Y-TZP老化后TP均值最低(7.05±0.261)。热液老化前后两种Y-TZP类型存在显著差异。XRD分析表明,时效后两种Y-TZP表面的单斜晶含量均有所增加。结论:单片Y-TZP的低温降解率高于芯型,这可能会显著影响半透明Y-TZP的外观和透明度,从而影响其耐久性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

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Translucency of monolithic and core zirconia after hydrothermal aging.

Objective: To evaluate the hydrothermal aging effect on the translucency of partially stabilized tetragonal zirconia with yttria (Y-TZP) used as monolithic or fully milled zirconia and of core type. Methods: Twenty disc-shaped specimens (1 and 10 mm) for each type of monolithic and core Y-TZP materials were milled and sintered according to the manufacturer's instruction. The final specimens were divided into two groups according to the type of Y-TZP used. Translucency parameter (TP) was measured over white and black backgrounds with the diffuse reflectance method; X-ray diffraction (XRD) and scanning electron microscope (SEM) were used to analyze the microstructure of both Y-TZP types before and after aging. Data for TP values was statistically analyzed using Student's t-test. Results: Monolithic Y-TZP showed the highest TP mean value (16.4 ± 0.316) before aging while core Y-TZP showed the lowest TP mean value (7.05 ± 0.261) after aging. There was a significant difference between the two Y-TZP types before and after hydrothermal aging. XRD analysis showed increases in monoclinic content in both Y-TZP surfaces after aging. Conclusion: Monolithic Y-TZP has a higher chance to low-temperature degradation than core type, which may significantly affect the esthetic appearance and translucency hence durability of translucent Y-TZP.

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