纳米杂化和杂化复合材料湿、干贮存60天的断裂韧性。

Journal of Dental Biomaterial Pub Date : 2017-03-01
M Sookhakiyan, S Tavana, Y Azarnia, R Bagheri
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引用次数: 0

摘要

问题陈述:患者对后牙区牙色修复体的需求正在增加。临床医生使用通用的纳米混合树脂复合材料的前和后区域。比较非杂化材料和杂化材料干湿储存的断裂韧性的报道很少。目的:通过四点弯曲试验,研究三种纳米杂化材料的断裂韧性,并将其与混合树脂复合材料干燥或湿储存60天的断裂韧性进行比较。材料与方法:采用四种树脂复合材料:三种纳米复合材料;Filtek Supreme (3M)、Ice (SDI)、TPH3 (Dentsply)和一种混合型Filtek P60 (3M)。每种材料制备40个尺寸为30 mm × 5mm × 2mm的矩形缺口梁试件。将标本随机分为4组(n = 10),分别在37℃蒸馏水和干燥条件下保存1和60 d。将试样置于四点试验夹具上,在万能试验机上以0.5mm/min的十字速度加载力(N),记录试样破坏时的最大载荷并计算KIC。结果:三因素方差分析显示各因素之间存在显著的交互作用(p < 0.0001)。除TPH3外,所有材料干燥贮藏的KIC均显著高于湿贮藏(p < 0.05)。干储1 d后,Ice的KIC最高(2.04±0.32),Filtek P60次之,Filtek Supreme最低(1.39±0.13),时间对断裂韧性的影响与材料有关。结论:湿储存对几乎所有材料的断裂韧性都有不利影响。保持修复体口中干燥可以增加其断裂韧性。因此,在修复体表面使用涂层剂可以防止其早期吸水,并在一段时间内增加其强度。
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Fracture Toughness of Nanohybrid and Hybrid Composites Stored Wet and Dry up to 60 Days.

Statement of problem: Patients' demand for tooth-colored restoratives in the posterior region is increasing. Clinicians use universal nanohybrid resin composites for both anterior and posterior regions. There are few published reports comparing fracture toughness of nonohybrids and that of hybrid composite stored wet and dry.

Objectives: To investigate the fracture toughness of three nanohybrids compared to that of a hybrid resin composite stored dry or wet up to 60 days, using four-point bending test.

Materials and methods: Four resin composites were used: three nanohybrids; Filtek Supreme (3M), Ice (SDI), TPH3 (Dentsply) and one hybrid Filtek P60 (3M). For each material, 40 rectangular notched beam specimens were prepared with dimensions of 30 mm × 5mm × 2mm. The specimens were randomly divided into 4 groups (n = 10) and stored at 37ºC either in distilled water or dry for 1 and 60 days. The specimens were placed on the four-point test jig and subjected to force (N) using universal testing machine loaded at a crosshead speed of 0.5mm/min and maximum load at specimen failure was recorded and KIC was calculated.

Results: Three-way ANOVA showed a significant interaction between all the factors (all p < .0001). Except for TPH3, all tested materials showed significantly higher KIC when stored dry than stored wet (p < 0.05). After 1 day of dry storage, Ice showed the highest KIC (2.04± 0.32) followed by Filtek P60 and the lowest was for Filtek Supreme (1.39± 0.13) The effect of time on fracture toughness was material dependent.

Conclusions: Wet storage adversely affected the fracture toughness of almost all materials. Keeping the restoration dry in the mouth may increase their fracture toughness. Therefore, using a coating agent on the surface of restoration may protect them from early water uptake and increase their strength during a time period.

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