桂花根化学成分黄酮类化合物研究

中药材 Pub Date : 2016-07-01

Wei Yin, Jin-qi Liu

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引用次数: 0

摘要

目的:研究桂花根的化学成分。方法:采用硅胶、Sephadex LH-20等材料对桂花根醇提液进行分离纯化，通过理化性质和波谱分析对其结构进行鉴定。结果:从桂花根中分离到13种黄酮类化合物，分别为:光酚(1)、二氢槲皮素(2)、2′-羟基-5,7,8-三甲氧基黄酮(3)、羽花素(4)、根黄素(5)、芹菜素(6)、花萼黄素(7)、槲皮素(8)、3′，4′，5,7-四羟基黄酮(9)、5′-7,8,2′，6′-四甲基黄酮(10)、异槲皮素(11)、金盏花素(12)、山母酚(13)。结论:化合物1 ~ 5、7、9 ~ 12为首次从桂花中分离得到。

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[The Flavonoids of Chemical Constituents of Osmanthus fragrans Roots].

Objective: To investigate the constituents of the roots in Osmanthus fragrans.

Methods: The Osmanthus fragrans roots alcohol extract solution were separated and purified by silica gel,Sephadex LH-20 and other materials, the structures were identified by physicochemical properties and spectral analysis.

Results: Thirteen flavonoids were isolated from the roots of Osmanthus fragrans,which identified as glabrol ( 1), dihydroquercetin( 2),2’-hydroxy-5,7,8-trimethoxyflavone( 3),lupinifolin( 4), phloretin( 5), apigenin ( 6), calycosine( 7), quercetin( 8),3’,4’,5,7-tetrahydroxy flavanone( 9),5-hydroxy-7,8,2’,6’-tetramethoxyflavone( 10),isoliquiritigenin( 11),tonkinensisol( 12),kaempferol ( 13).

Conclusion: Compounds 1 ~ 5,7,9 ~ 12 are isolated from the Osmanthus fragrans for the first time.

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来源期刊

中药材

自引率

0.00%

发文量

11364

期刊介绍： "Chinese Materia Medica" magazine was founded in 1978. It is a national-level academic journal of Chinese medicine science and technology approved by the State Science and Technology Commission and the Press and Publication Administration for public distribution at home and abroad. It is sponsored by the Chinese Materia Medica Information Center of the State Food and Drug Administration and is publicly distributed at home and abroad. It mainly reports on new technologies, new methods and new achievements in the production, scientific research and business management of Chinese medicine, and serves to promote the production and scientific and technological development of Chinese medicine, improve the output and quality of Chinese medicine, improve business management, and prosper the Chinese medicine industry.