{"title":"外消旋n -烷基化巴比妥酸酯的对映选择性气相色谱分离:C11-Chirasil-Dex作为GC手性固定相的应用。","authors":"Ashraf Ghanem","doi":"","DOIUrl":null,"url":null,"abstract":"<p><p>Chirasil-beta-Dex containing an undecamethylene spacer (C11-Chirasil-Dex) was synthesized and used as chiral stationary phase (CSP) in enantioselective gas chromatography (GC). The versatility of the new stationary phase in the simultaneous enantiomeric separation of a set of N-alkylated barbiturates is demonstrated.</p>","PeriodicalId":7781,"journal":{"name":"Analytical Chemistry Insights","volume":"2 ","pages":"75-80"},"PeriodicalIF":0.0000,"publicationDate":"2007-09-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2716807/pdf/","citationCount":"0","resultStr":"{\"title\":\"Enantioselective gas chromatographic separation of racemic N-alkylated barbiturates: application of C11-Chirasil-Dex as chiral stationary phase in GC.\",\"authors\":\"Ashraf Ghanem\",\"doi\":\"\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p><p>Chirasil-beta-Dex containing an undecamethylene spacer (C11-Chirasil-Dex) was synthesized and used as chiral stationary phase (CSP) in enantioselective gas chromatography (GC). The versatility of the new stationary phase in the simultaneous enantiomeric separation of a set of N-alkylated barbiturates is demonstrated.</p>\",\"PeriodicalId\":7781,\"journal\":{\"name\":\"Analytical Chemistry Insights\",\"volume\":\"2 \",\"pages\":\"75-80\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2007-09-18\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2716807/pdf/\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Analytical Chemistry Insights\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Analytical Chemistry Insights","FirstCategoryId":"1085","ListUrlMain":"","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Enantioselective gas chromatographic separation of racemic N-alkylated barbiturates: application of C11-Chirasil-Dex as chiral stationary phase in GC.
Chirasil-beta-Dex containing an undecamethylene spacer (C11-Chirasil-Dex) was synthesized and used as chiral stationary phase (CSP) in enantioselective gas chromatography (GC). The versatility of the new stationary phase in the simultaneous enantiomeric separation of a set of N-alkylated barbiturates is demonstrated.
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