在长期储存的改进碘化物配方中,与羟基自由基生成相关的特定dpo - oh加合物信号的形成。

IF 0.9 4区 农林科学 Q4 BIOTECHNOLOGY & APPLIED MICROBIOLOGY Biocontrol science Pub Date : 2022-01-01 DOI:10.4265/bio.27.47
Nori Kida
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引用次数: 0

摘要

采用电子自旋共振(ESR)技术,在pH为0.3的FeCl3、EDTA、KI和乙醇溶液中制备的KMT试剂中,发现了与羟基自由基生成相关的DMPO-OH加合物信号(1:2:2:1)。虽然N,N,N,N,N,N-四甲基-对苯二胺(TMPD)和N,N-二乙基-对苯二胺(DPD)的颜色强度不同,但长期储存的蒸馏KMT试剂和TMPD的混合物呈现出类似伍斯特蓝的紫色,而长期储存的蒸馏KMT试剂和DPD的混合物呈现出类似伍斯特红的粉红色。长期储存的蒸馏KMT试剂有可能具有生成羟基自由基的能力。
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Formation of a Specific DMPO-OH Adduct Signal Related to Hydroxy Radical Generation in a Long Term Stored Improved Iodide Formulation.

A specific DMPO-OH adduct signal (1:2:2:1)related to hydroxyl radical generation in a longterm stored improved iodide formulation, tentatively designated as the distilled KMT reagent which prepared from a pH 0.3 solution containing FeCl3, EDTA, KI and ethanol termed the KMT reagent, was detected by electron spin resonance (ESR) spectroscopy.Although the color intensities of N,N,N,N-tetramethyl-p-phenylenediamine (TMPD) and N,N-diethyl-p-phenylenediamine (DPD) differ, the mixture of the long-term stored distilled KMT reagent and TMPD exhibited a purple color similar to Wurster's blue, and the mixture of the long-term stored distilled KMT reagent and DPD exhibited a pink color similar to Wurster's red. There is a possibility that the long-term stored distilled KMT reagent may possess with the ability to generate a hydroxyl radical.

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来源期刊
Biocontrol science
Biocontrol science BIOTECHNOLOGY & APPLIED MICROBIOLOGY-
CiteScore
2.60
自引率
8.30%
发文量
21
审稿时长
>12 weeks
期刊介绍: The Biocontrol Science provides a medium for the publication of original articles, concise notes, and review articles on all aspects of science and technology of biocontrol.
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