紫茉莉提取物制备银/TiO2纳米颗粒及表征

F. O. Purnomo, S. S. Ningrum, Sadwika Najmi Kautsari
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引用次数: 0

摘要

绿色合成纳米材料以其低毒、低能耗、环保、高效、廉价、无污染等特点得到了广泛的发展。利用紫茉莉植物提取物进行了银掺杂二氧化钛纳米颗粒(Ag/TiO2-NPs)的绿色合成。植物提取物被用作还原剂。通过FT-IR、FESEM和XRD对合成的Ag/TiO2纳米颗粒的官能团、形貌和晶体结构进行了研究。FESEM分析证实,Ag/TiO2纳米颗粒的形态为球形,平均尺寸约为400nm。Ag/TiO2 NP的晶粒尺寸通过Scherrer公式计算,并且发现平均尺寸在15.72nm的范围内。XRD分析结果显示锐钛矿和金红石相中的金属银和TiO2颗粒的fcc结构。
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Synthesis and Characterization of Ag/TiO2 Nanoparticles using Mirabilis jalapa Plant Extract
Green synthesized nanomaterials have been widely developed because of their less toxicity, low energy process, environmentally friendly, effective, cheap, and pollution-free. Green synthesis of silver doped titanium dioxide nanoparticles (Ag/TiO2 NPs) was carried out using Mirabilis jalapa plant extract. The plant extract was used as a reducing agent. The functional groups, morphology, and crystalline structure of as-synthesized Ag/TiO2 NPs were investigated by FT-IR, FESEM, and XRD. Analysis by FESEM confirmed that the morphology of Ag/TiO2 NPs is spherical with an average size of ~ 400 nm. Crystallite size for the Ag/TiO2 NPs was calculated by the Scherrer formula dan the average size found to be in the range of 15.72 nm. The result of XRD analysis showing the fcc structure for metallic silver and TiO2 particles in the anatase and rutile phases.
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CiteScore
0.80
自引率
0.00%
发文量
15
审稿时长
24 weeks
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