碱性介质中溶胶-凝胶法合成Zn-O纳米颗粒及其光学性能

Pub Date : 2022-04-01 DOI:10.15251/jobm.2022.142.69
D. Tamilselvi, N. Velmani, K. Rathidevi, V. Geethalakshmi, R. Nandhini
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引用次数: 0

摘要

以ZnSO4.7H2O为前驱体,在碱性介质中通过溶胶-凝胶法成功合成了Zn-O纳米颗粒。分析了Zn-O纳米颗粒的结构、形态和光学性质。利用X射线衍射(XRD)、傅立叶变换红外光谱(FTIR)、紫外可见分光光度计、扫描电子显微镜(SEM)和能量分散X射线分析(EDAX)对Zn-O纳米粒子进行了表征。扫描电子显微镜(SEM)观察显示Zn-O NPs的形态结构发生了显著变化。分析研究证实了合成的Zn-O纳米颗粒中存在的官能团和化学键。
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Synthesis, characterization with optical property of Zn-O NPs using sol-gel route in alkaline medium
Zn-O nanoparticles were successfully synthesized by sol-gel route using ZnSO4.7H2O as precursor in alkaline medium. Structural, morphological and optical property of Zn-O NPs was analyzed. Zn-O NPs were characterized by using X-ray diffraction (XRD), Fourier transform infrared spectral (FTIR), UV-Visible spectrophotometer, scanning electron microscopy (SEM) and Energy Dispersive X-ray analysis (EDAX).XRD pattern shows the purity of synthesized Zn-O nanoparticles particle size. Scanning electron microscopy (SEM) observations revealed remarkable change in morphological structure of Zn-O NPs. Analysis studies was confirmed, the functional groups and chemical bonding present in the synthesized Zn-O nanoparticles.
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