Y. Ikoma, T. Yamasaki, T. Masuda, Y. Tange, Y. Higo, Y. Ohishi, M. McCartney, David J. Smith, Z. Horita
{"title":"高压扭转硅退火过程中相变的同步X射线衍射观察","authors":"Y. Ikoma, T. Yamasaki, T. Masuda, Y. Tange, Y. Higo, Y. Ohishi, M. McCartney, David J. Smith, Z. Horita","doi":"10.1080/09500839.2021.1905192","DOIUrl":null,"url":null,"abstract":"ABSTRACT In situ observation of a phase transformation during annealing of Si containing diamond-cubic (dc) and metastable phases has been performed using synchrotron X-ray diffraction. Metastable body-centred-cubic (bc8) and rhombohedral (r8) phases were formed by high-pressure torsion. These metastable phases gradually disappeared when increasing the annealing temperature to ∼ 180°C while another metastable phase having a hexagonal diamond (hd) structure appeared at ∼ 190°C. High-resolution transmission microscopy analysis revealed that hd and dc grains were present after annealing at 200°C. The results indicate that a phase transformation, mainly from bc8 to hd, occurred during annealing.","PeriodicalId":19860,"journal":{"name":"Philosophical Magazine Letters","volume":"101 1","pages":"223 - 231"},"PeriodicalIF":1.2000,"publicationDate":"2021-04-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/09500839.2021.1905192","citationCount":"2","resultStr":"{\"title\":\"Synchrotron X-ray diffraction observation of phase transformation during annealing of Si processed by high-pressure torsion\",\"authors\":\"Y. Ikoma, T. Yamasaki, T. Masuda, Y. Tange, Y. Higo, Y. Ohishi, M. McCartney, David J. Smith, Z. Horita\",\"doi\":\"10.1080/09500839.2021.1905192\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"ABSTRACT In situ observation of a phase transformation during annealing of Si containing diamond-cubic (dc) and metastable phases has been performed using synchrotron X-ray diffraction. Metastable body-centred-cubic (bc8) and rhombohedral (r8) phases were formed by high-pressure torsion. These metastable phases gradually disappeared when increasing the annealing temperature to ∼ 180°C while another metastable phase having a hexagonal diamond (hd) structure appeared at ∼ 190°C. High-resolution transmission microscopy analysis revealed that hd and dc grains were present after annealing at 200°C. The results indicate that a phase transformation, mainly from bc8 to hd, occurred during annealing.\",\"PeriodicalId\":19860,\"journal\":{\"name\":\"Philosophical Magazine Letters\",\"volume\":\"101 1\",\"pages\":\"223 - 231\"},\"PeriodicalIF\":1.2000,\"publicationDate\":\"2021-04-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1080/09500839.2021.1905192\",\"citationCount\":\"2\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Philosophical Magazine Letters\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.1080/09500839.2021.1905192\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Philosophical Magazine Letters","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.1080/09500839.2021.1905192","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
Synchrotron X-ray diffraction observation of phase transformation during annealing of Si processed by high-pressure torsion
ABSTRACT In situ observation of a phase transformation during annealing of Si containing diamond-cubic (dc) and metastable phases has been performed using synchrotron X-ray diffraction. Metastable body-centred-cubic (bc8) and rhombohedral (r8) phases were formed by high-pressure torsion. These metastable phases gradually disappeared when increasing the annealing temperature to ∼ 180°C while another metastable phase having a hexagonal diamond (hd) structure appeared at ∼ 190°C. High-resolution transmission microscopy analysis revealed that hd and dc grains were present after annealing at 200°C. The results indicate that a phase transformation, mainly from bc8 to hd, occurred during annealing.
期刊介绍：
Philosophical Magazine Letters is the rapid communications part of the highly respected Philosophical Magazine, which was first published in 1798. Its Editors consider for publication short and timely contributions in the field of condensed matter describing original results, theories and concepts relating to the structure and properties of crystalline materials, ceramics, polymers, glasses, amorphous films, composites and soft matter. Articles emphasizing experimental, theoretical and modelling studies on solids, especially those that interpret behaviour on a microscopic, atomic or electronic scale, are particularly appropriate.
Manuscripts are considered on the strict condition that they have been submitted only to Philosophical Magazine Letters , that they have not been published already, and that they are not under consideration for publication elsewhere.
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