Atefeh Ghasemi, A. Davoodnia, M. Pordel, N. Tavakoli-Hoseini
{"title":"负载在SiO2上的P2O5作为一种高效且可重复使用的催化剂在无溶剂条件下快速一锅合成氨基甲酸烷基萘酚","authors":"Atefeh Ghasemi, A. Davoodnia, M. Pordel, N. Tavakoli-Hoseini","doi":"10.1080/23312009.2017.1317582","DOIUrl":null,"url":null,"abstract":"Abstract Under mild conditions and without any additional organic solvent, synthesis of carbamatoalkyl naphthols by the one-pot three-component reaction of β-naphthol with a wide range of aromatic aldehydes and methyl carbamate could be carried out in the presence of P2O5 supported on SiO2 (P2O5/SiO2). The results showed that the catalyst has high activity and the desired products were obtained in high yields in short reaction times. Other beneficial features of this protocol include inexpensive and easily obtained catalyst, simple work-up, and the recyclability and reusability of the catalyst for up to five consecutive runs.","PeriodicalId":10640,"journal":{"name":"Cogent Chemistry","volume":" ","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1080/23312009.2017.1317582","citationCount":"3","resultStr":"{\"title\":\"P2O5 supported on SiO2 as an efficient and reusable catalyst for rapid one-pot synthesis of carbamatoalkyl naphthols under solvent-free conditions\",\"authors\":\"Atefeh Ghasemi, A. Davoodnia, M. Pordel, N. Tavakoli-Hoseini\",\"doi\":\"10.1080/23312009.2017.1317582\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Abstract Under mild conditions and without any additional organic solvent, synthesis of carbamatoalkyl naphthols by the one-pot three-component reaction of β-naphthol with a wide range of aromatic aldehydes and methyl carbamate could be carried out in the presence of P2O5 supported on SiO2 (P2O5/SiO2). The results showed that the catalyst has high activity and the desired products were obtained in high yields in short reaction times. Other beneficial features of this protocol include inexpensive and easily obtained catalyst, simple work-up, and the recyclability and reusability of the catalyst for up to five consecutive runs.\",\"PeriodicalId\":10640,\"journal\":{\"name\":\"Cogent Chemistry\",\"volume\":\" \",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2017-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1080/23312009.2017.1317582\",\"citationCount\":\"3\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Cogent Chemistry\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1080/23312009.2017.1317582\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Cogent Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1080/23312009.2017.1317582","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
P2O5 supported on SiO2 as an efficient and reusable catalyst for rapid one-pot synthesis of carbamatoalkyl naphthols under solvent-free conditions
Abstract Under mild conditions and without any additional organic solvent, synthesis of carbamatoalkyl naphthols by the one-pot three-component reaction of β-naphthol with a wide range of aromatic aldehydes and methyl carbamate could be carried out in the presence of P2O5 supported on SiO2 (P2O5/SiO2). The results showed that the catalyst has high activity and the desired products were obtained in high yields in short reaction times. Other beneficial features of this protocol include inexpensive and easily obtained catalyst, simple work-up, and the recyclability and reusability of the catalyst for up to five consecutive runs.