曼陀罗合成植物微量元素含银纳米颗粒的光谱分析。

Q4 Environmental Science Indonesian Journal of Biotechnology Pub Date : 2023-06-27 DOI:10.22146/ijbiotech.76257
Gurushankar Krishnamoorthy, K. Chinnaiah, K. Kannan, V. Maik, V. Potemkin, M. Grishina, S. Christopher Jeyaseelan, A. Muthuvel, D. Gnanasangeetha
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引用次数: 1

摘要

本文以曼陀罗叶提取物为原料,采用绿色合成方法制备了纳米银。曼陀罗是茄科的一种中草药。采用UV-Vis光谱仪、x射线衍射仪(XRD)、傅里叶变换红外光谱仪(FTIR)和扫描电子显微镜(SEM)及能量色散x射线分析(EDAX)技术对制备的Ag NPs进行了表征。在415 nm处出现表面等离子体共振(SPR)峰,表明银纳米粒子在紫外可见光谱中产生。XRD谱图显示了银纳米粒子的面心立方晶体结构,具有有机金属配合物相。FTIR光谱中的峰显示生物分子的存在。SEM图像说明了其碎屑岩形态,EDAX剖面证实了银和植物微量元素的存在。对制备的银电极进行了循环伏安法(CV)、氯离子电位法(choronpotential)和电化学阻抗谱(EIS)分析。在0.5 A/g下的比电容为267.59 F/g,充放电5000次后的循环保持率为83.7%。因此,这种材料可以用作超级电容器储能装置。
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Spectroscopic analysis of plant trace element incorporated silver nanoparticles synthesis from Datura metel l.
Here in we report, silver nanoparticles (Ag NPs) prepared from leaf extract of Datura metel L. via green synthesis method. Datura metel L. is an herbal medicinal plant of solanaceae family. The as - prepared Ag NPs characterized employing UV-Vis spectrometer, X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy and scanning electron microscopy (SEM) with energy dispersive X-ray analysis (EDAX) techniques. The appearance of Surface Plasmon Resonance (SPR) peak at 415 nm suggested that creation of Ag NPs in UV-Vis spectrum. XRD pattern showed face centered cubic crystal structure of Ag NPs with organometallic complex phase. Peaks in FTIR spectrum reveal the existence of biomolecules. SEM image illustrate their clastic rock morphology and EDAX profile authenticate the company of Ag and plant trace element. The Cyclic voltammetry (CV), Choronopotentiometry, and Electrochemical impedance spectroscopy (EIS) analysis were performed as prepared Ag electrode. The specific capacitance of 267.59 F/g at 0.5 A/g and cyclic retention of 83.7% after charge-discharge 5000 cycles are obtained. Hence this material could be utilized as Supercapacitor energy storage devices.
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来源期刊
Indonesian Journal of Biotechnology
Indonesian Journal of Biotechnology Environmental Science-Environmental Science (miscellaneous)
CiteScore
1.00
自引率
0.00%
发文量
20
审稿时长
12 weeks
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