Tapiero-Cuellar Jose Libardo, Guillermo Salamanca-Grosso, M. Benitez
{"title":"微波辅助液压蒸馏法提取哥伦比亚姜精油挥发物及抗氧化活性分析","authors":"Tapiero-Cuellar Jose Libardo, Guillermo Salamanca-Grosso, M. Benitez","doi":"10.23850/24220582.3465","DOIUrl":null,"url":null,"abstract":"The (Zingiber officinale) is a plant of the zingiberáceas family, its rhizome is widely used in gastronomy for its pungent aroma and flavor. Essential oils (EO) are natural compounds; they have 25 to 70 components with different concentrations. Α-Zingiberene and α-Felandrene are the main components with volumes between 20% and 70%. For the extraction of the AE samples from 10 Colombian geographical locations were used, obtained by microwave radiated hydrodistillation (MWHD) and stored at 4°C in amber vials. 50 µL of EA and 1.0 µL of (n-tetradecane) internal standard were dissolved in dichloromethane to a final volume of 1.0 mL. The EO components were performed on a triple quadruple mass detector gas chromatograph (BRUKER 450GC-320). For its antioxidant activity (AA) the methodology of Prior for DPPH* and ABTS+ was used. The extractions showed a yield between 0.053 and 0.109 percent; and 300 g of sample at 700 watts and 40 minutes of process were used. The chromatographic profile showed 43 components referring to ketones, alcohols, cyclic ethers, aldehydes and 23 hydrocarbons, with α-Zingiberene being the majority, considered as a molecular marker of this EO. The AA presents significant differences between the samples evaluated for the localities studied.","PeriodicalId":40198,"journal":{"name":"Revista Colombiana de Investigaciones Agroindustriales","volume":null,"pages":null},"PeriodicalIF":0.4000,"publicationDate":"2021-06-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Analysis of volatile compounds and antioxidant activity of Colombian ginger (Zingiber officinale) essential oil obtained by hydrohydraulic distillation assisted by microwave radiation\",\"authors\":\"Tapiero-Cuellar Jose Libardo, Guillermo Salamanca-Grosso, M. Benitez\",\"doi\":\"10.23850/24220582.3465\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The (Zingiber officinale) is a plant of the zingiberáceas family, its rhizome is widely used in gastronomy for its pungent aroma and flavor. Essential oils (EO) are natural compounds; they have 25 to 70 components with different concentrations. Α-Zingiberene and α-Felandrene are the main components with volumes between 20% and 70%. For the extraction of the AE samples from 10 Colombian geographical locations were used, obtained by microwave radiated hydrodistillation (MWHD) and stored at 4°C in amber vials. 50 µL of EA and 1.0 µL of (n-tetradecane) internal standard were dissolved in dichloromethane to a final volume of 1.0 mL. The EO components were performed on a triple quadruple mass detector gas chromatograph (BRUKER 450GC-320). For its antioxidant activity (AA) the methodology of Prior for DPPH* and ABTS+ was used. The extractions showed a yield between 0.053 and 0.109 percent; and 300 g of sample at 700 watts and 40 minutes of process were used. The chromatographic profile showed 43 components referring to ketones, alcohols, cyclic ethers, aldehydes and 23 hydrocarbons, with α-Zingiberene being the majority, considered as a molecular marker of this EO. The AA presents significant differences between the samples evaluated for the localities studied.\",\"PeriodicalId\":40198,\"journal\":{\"name\":\"Revista Colombiana de Investigaciones Agroindustriales\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.4000,\"publicationDate\":\"2021-06-08\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Revista Colombiana de Investigaciones Agroindustriales\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.23850/24220582.3465\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"AGRICULTURE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Revista Colombiana de Investigaciones Agroindustriales","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.23850/24220582.3465","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"AGRICULTURE, MULTIDISCIPLINARY","Score":null,"Total":0}
Analysis of volatile compounds and antioxidant activity of Colombian ginger (Zingiber officinale) essential oil obtained by hydrohydraulic distillation assisted by microwave radiation
The (Zingiber officinale) is a plant of the zingiberáceas family, its rhizome is widely used in gastronomy for its pungent aroma and flavor. Essential oils (EO) are natural compounds; they have 25 to 70 components with different concentrations. Α-Zingiberene and α-Felandrene are the main components with volumes between 20% and 70%. For the extraction of the AE samples from 10 Colombian geographical locations were used, obtained by microwave radiated hydrodistillation (MWHD) and stored at 4°C in amber vials. 50 µL of EA and 1.0 µL of (n-tetradecane) internal standard were dissolved in dichloromethane to a final volume of 1.0 mL. The EO components were performed on a triple quadruple mass detector gas chromatograph (BRUKER 450GC-320). For its antioxidant activity (AA) the methodology of Prior for DPPH* and ABTS+ was used. The extractions showed a yield between 0.053 and 0.109 percent; and 300 g of sample at 700 watts and 40 minutes of process were used. The chromatographic profile showed 43 components referring to ketones, alcohols, cyclic ethers, aldehydes and 23 hydrocarbons, with α-Zingiberene being the majority, considered as a molecular marker of this EO. The AA presents significant differences between the samples evaluated for the localities studied.