{"title":"溶液燃烧合成氧硼酸铁（Fe3BO6）","authors":"D. Ozer, O. Icten","doi":"10.18596/JOTCSA.500355","DOIUrl":null,"url":null,"abstract":"In this study, iron oxyborate (Fe 3 BO 6 ) was first synthesized through solution combustion method as a potential anode material for lithium-ion batteries. Urea, glycine, citric acid, carbohydrazide, hexamethylene tetramine, and starch were used as fuel sources and the effects of fuels were investigated. The obtained materials were structurally characterized by FT-IR, powder-XRD and solid UV-Vis. The pure crystalline Fe 3 BO 6 was synthesized at low temperature and short reaction time using glycine assisted solution combustion method. It was thermally stable up to 945 °C with non-uniform morphology and a highly porous structure. The magnetic properties were also studied and Fe 3 BO 6 show antiferromagnetic behavior.","PeriodicalId":17402,"journal":{"name":"Journal of the Turkish Chemical Society, Section A: Chemistry","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2019-06-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"4","resultStr":"{\"title\":\"Solution Combustion Synthesis of Iron Oxyborate (Fe3BO6)\",\"authors\":\"D. Ozer, O. Icten\",\"doi\":\"10.18596/JOTCSA.500355\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this study, iron oxyborate (Fe 3 BO 6 ) was first synthesized through solution combustion method as a potential anode material for lithium-ion batteries. Urea, glycine, citric acid, carbohydrazide, hexamethylene tetramine, and starch were used as fuel sources and the effects of fuels were investigated. The obtained materials were structurally characterized by FT-IR, powder-XRD and solid UV-Vis. The pure crystalline Fe 3 BO 6 was synthesized at low temperature and short reaction time using glycine assisted solution combustion method. It was thermally stable up to 945 °C with non-uniform morphology and a highly porous structure. The magnetic properties were also studied and Fe 3 BO 6 show antiferromagnetic behavior.\",\"PeriodicalId\":17402,\"journal\":{\"name\":\"Journal of the Turkish Chemical Society, Section A: Chemistry\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2019-06-15\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"4\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of the Turkish Chemical Society, Section A: Chemistry\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.18596/JOTCSA.500355\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"Chemistry\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of the Turkish Chemical Society, Section A: Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.18596/JOTCSA.500355","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"Chemistry","Score":null,"Total":0}
Solution Combustion Synthesis of Iron Oxyborate (Fe3BO6)
In this study, iron oxyborate (Fe 3 BO 6 ) was first synthesized through solution combustion method as a potential anode material for lithium-ion batteries. Urea, glycine, citric acid, carbohydrazide, hexamethylene tetramine, and starch were used as fuel sources and the effects of fuels were investigated. The obtained materials were structurally characterized by FT-IR, powder-XRD and solid UV-Vis. The pure crystalline Fe 3 BO 6 was synthesized at low temperature and short reaction time using glycine assisted solution combustion method. It was thermally stable up to 945 °C with non-uniform morphology and a highly porous structure. The magnetic properties were also studied and Fe 3 BO 6 show antiferromagnetic behavior.
京公网安备 11010802042870号
京ICP备2023020795号-1
分享
求助内容：
应助结果提醒方式：
扫码关注我们
