氩弧等离子炬净化片状石墨的研究

Q4 Engineering 强激光与粒子束 Pub Date : 2021-06-15 DOI:10.11884/HPLPB202133.210118
Cheng Yue, Yu Zhe, Li Jinmao, Song Chunlian, Zhao Zhihao, Lu Dandan, Zhang Xiaofang
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引用次数: 2

摘要

纯度在99.9%以上的高纯石墨,作为一种工业原料,在高新技术领域发挥着重要作用。现有的物理和化学方法提纯石墨工艺成本高、酸碱对设备和环境破坏严重、工艺复杂。因此,开发一种优良有效的石墨净化技术已成为近年来国内外的研究热点。建立了一种用电弧等离子体提纯片状石墨的方法。利用电弧等离子体快速产生高温的特点,对黑龙江省鸡西市纯度为94.18%的片状石墨样品进行高温处理。结果表明,最优放电参数为风量25 L/min、电流400 A、功率10 kW。此时,电弧等离子体的表面温度高达3350℃。利用扫描电子显微镜对电弧处理前后石墨样品的微观结构进行对比,找出石墨样品的切碎破碎特征。按GB/T 3521 2008国家标准化学分析方法对石墨纯度和杂质进行分析。经电弧处理后,石墨纯度提高到99.21%。
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Study on purification of flaky graphite by argon arc plasma torch
High purity graphite with purity above 99.9%, as an industrial raw material, plays an important role in the high-tech field. The existing physical and chemical methods of graphite purification technology has high cost serious damage to equipment and environment by acid and alkali, and complex processes. Thus the development of an excellent and effective graphite purification technology has become a research hotspot in recent years at home and abroad. A purification method of flaky graphite by arc plasma is established in this paper. The characteristics of high temperature which can be produced quickly by using arc plasma is used to treat the flaky graphite samples with a purity of 94.18% from Jixi City of Heilongjiang Province, under high temperature. The results show that the optimal discharge parameters are air flow rate 25 L/min, current 400 A and power 10 kW. At this point, the surface temperature of the arc plasma is up to 3350 ℃. Scanning electron microscope is used to compare the microstructure of graphite samples before and after arc processing to find the characteristics of shredding and breaking of graphite samples. The graphite purity and impurities are analysed according to national standard chemical analysis method of GB/T 3521 2008. After arc treatment, the purity of graphite is increased to 99.21%.
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来源期刊
强激光与粒子束
强激光与粒子束 Engineering-Electrical and Electronic Engineering
CiteScore
0.90
自引率
0.00%
发文量
11289
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