建立了“乙醇为内标法”直接测定酒精产品中挥发性物质的计量特性

IF 1.8 Q3 CHEMISTRY, ANALYTICAL Journal of Chemical Metrology Pub Date : 2018-06-06 DOI:10.25135/JCM.14.18.02.063
S. Charapitsa, S. Sytova, Anton Korban, Nicolai Boyarin, I. Shestakovich, R. Čabala
{"title":"建立了“乙醇为内标法”直接测定酒精产品中挥发性物质的计量特性","authors":"S. Charapitsa, S. Sytova, Anton Korban, Nicolai Boyarin, I. Shestakovich, R. Čabala","doi":"10.25135/JCM.14.18.02.063","DOIUrl":null,"url":null,"abstract":"An extensive study concerning the problem of volatile compounds determination in alcoholic products by gas chromatography has been undertaken in the paper. A row of gravimetrically prepared standard solutions was analysed with three analytical methods: traditional method of internal standard, advanced method of internal standard and external standard method. The main analytical characteristics and metrological parameters of the “Ethanol as Internal Standard” method were compared with the traditional approaches. It was shown that this method leads to correct values of volatiles concentrations and the corresponding metrological characteristics are generally better.","PeriodicalId":15343,"journal":{"name":"Journal of Chemical Metrology","volume":" ","pages":""},"PeriodicalIF":1.8000,"publicationDate":"2018-06-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"12","resultStr":"{\"title\":\"The establishment of metrological characteristics of the method “Ethanol as Internal Standard” for the direct determination of volatile compounds in alcoholic products\",\"authors\":\"S. Charapitsa, S. Sytova, Anton Korban, Nicolai Boyarin, I. Shestakovich, R. Čabala\",\"doi\":\"10.25135/JCM.14.18.02.063\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"An extensive study concerning the problem of volatile compounds determination in alcoholic products by gas chromatography has been undertaken in the paper. A row of gravimetrically prepared standard solutions was analysed with three analytical methods: traditional method of internal standard, advanced method of internal standard and external standard method. The main analytical characteristics and metrological parameters of the “Ethanol as Internal Standard” method were compared with the traditional approaches. It was shown that this method leads to correct values of volatiles concentrations and the corresponding metrological characteristics are generally better.\",\"PeriodicalId\":15343,\"journal\":{\"name\":\"Journal of Chemical Metrology\",\"volume\":\" \",\"pages\":\"\"},\"PeriodicalIF\":1.8000,\"publicationDate\":\"2018-06-06\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"12\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Chemical Metrology\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.25135/JCM.14.18.02.063\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"CHEMISTRY, ANALYTICAL\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Chemical Metrology","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.25135/JCM.14.18.02.063","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"CHEMISTRY, ANALYTICAL","Score":null,"Total":0}
引用次数: 12

摘要

本文对气相色谱法测定醇类产品中挥发性化合物的问题进行了广泛的研究。采用传统内标法、先进内标法和外标法三种分析方法对一排重量法配制的标准溶液进行了分析。将“乙醇内标法”的主要分析特性和计量参数与传统方法进行了比较。结果表明,该方法可以得到正确的挥发物浓度值,相应的计量特性通常较好。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
The establishment of metrological characteristics of the method “Ethanol as Internal Standard” for the direct determination of volatile compounds in alcoholic products
An extensive study concerning the problem of volatile compounds determination in alcoholic products by gas chromatography has been undertaken in the paper. A row of gravimetrically prepared standard solutions was analysed with three analytical methods: traditional method of internal standard, advanced method of internal standard and external standard method. The main analytical characteristics and metrological parameters of the “Ethanol as Internal Standard” method were compared with the traditional approaches. It was shown that this method leads to correct values of volatiles concentrations and the corresponding metrological characteristics are generally better.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
Journal of Chemical Metrology
Journal of Chemical Metrology CHEMISTRY, ANALYTICAL-
CiteScore
2.30
自引率
15.40%
发文量
7
期刊最新文献
Gradient reversed-phase HPLC method for the quantitation of azelnidipine and chlorthalidone in a fixed-dose synthetic mixture A new HPLC-UV method for the simultaneous measurements of α-escin and β-escin in creams containing Aesculus hippocastanum L. extract Quantification of main secondary metabolites of Satureja icarica P.H. Davis (Lamiaceae) by LC-HRMS and evaluation of antioxidant capacities An effective HPLC method for evaluation of process related impurities of Letermovir and LC-MS/MS characterization of forced degradation compounds A validated RP-HPLC assay method for Tofacitinib in pharmaceutical drug products
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1