高频电流处理下,结合𝑨 +𝑩 /𝑶𝟑based混合物加热的自传播高温合成硬化涂层的射线物相及显微组织分析

Q3 Engineering Eurasian Physical Technical Journal Pub Date : 2022-06-15 DOI:10.31489/2022no2/6-12
A. Ishkov
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引用次数: 0

摘要

本文介绍了自蔓延高温合成过程中获得的硬化硼化物涂层的研究结果。这些涂层是基于氧化铝和硼的复合材料。对获得的涂层进行X射线相和微观结构分析,显示了所得组合物的主要成分,并使评估涂层基底金属过渡区的厚度和结构成为可能。硅和铁的不同含量使得有可能评估在高频电流处理加热基础混合物样品时自蔓延高温合成过程中表面化学和冶金过程的发生。表明了将高频电流处理与自蔓延高温合成工艺相结合以获得更好质量的硬化涂层溅射的方便性。确定了涂层中具有不同厚度和涂层结构的两个区域的外观。
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RAY PHASE AND MICROSTRUCTURAL ANALYSIS OFHARDENING COATINGS OBTAINED BYSELF-PROPAGATING HIGH-TEMPERATURE SYNTHESIS IN COMBINATION WITH HEATING OFA MIXTURE OF 𝑨𝒍+𝑩𝟐𝑶𝟑BASED ON HIGH-FREQUENCY CURRENT TREATMENT
The paper describes the results of studies of hardening boride coatings obtained during the implementation of the process of self-propagating high-temperature synthesis. These coatings were composite materials based on aluminum oxide and boron. The obtained coatings were subjected to X-ray phase and microstructural analysis, which showed the maincomponents of the resulting compositions and made it possible to assess the thickness and structure of the coating-base metal transition area. The different content of silicon and iron makes it possible to assess the occurrence of surface chemical and metallurgical processes during self-propagating high-temperature synthesis when heating of the base mixture samples on high-frequency current treatment. The expediency of using high-frequency current treatment in combination with the process of self-propagating high-temperature synthesis for better-quality spattering of the hardening coating is shown. The appearance of two areas in the coating with different thickness and structure of the coating is established.
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发文量
15
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