NaCl盐对微波加氢蒸馏法提取柠檬叶精油的影响

IF 1 Q4 CHEMISTRY, MULTIDISCIPLINARY Indonesian Journal of Chemistry Pub Date : 2023-08-15 DOI:10.22146/ijc.78919
F. Suryanti, L. Qadariyah, M. Mahfud
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引用次数: 2

摘要

精油是从植物中提取并通过蒸馏获得的化合物。印尼有多种植物性商品用于生产精油。在印度尼西亚尚未开发的精油中,有一种是可以从柠檬草植物中提取的香茅油。在这项研究中,我们开发的微波加氢蒸馏(MHD)方法比传统蒸馏方法有几个优点:时间更短,油质和收率更高。本研究提出了用MHD法从柠檬草叶中提取香茅油,方法是添加水溶液和NaCl溶液。操作变量包括提取时间(20–180分钟)、材料尺寸(0.5、1.0和1.5厘米)、进料与溶剂的比例(0.1、0.15和0.2 g/mL)以及微波功率(300、450和600瓦)。通过GC-MS分析、比重、折射率和溶解度对精油的结果进行分析。结果表明,在几乎不变的条件下,它随着萃取时间的增加而增加,随着进料与溶剂比的增加而趋于减少,并且随着微波功率的增加而提高产率。GC-MS分析结果表明,香茅醛和香叶醇的有效成分含量分别为5.62%和46.61%。
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Effect of Addition of NaCl Salt on Extraction of Essential Oil from Lemongrass Leaves by Microwave Hydro-Distillation Method
Essential oils are compounds extracted from plants and obtained by distillation. Indonesia has many kinds of plant commodities for essential oil production. Among the essential oils that have not been developed in Indonesia is citronella oil which can be extracted from the lemongrass plant this research, we develop Microwave Hydro-Distillation (MHD) method has several advantages over conventional distillation methods: shorter time, higher oil quality and yield. This research proposes to extract citronella oil from lemongrass leaves using the MHD method using aquadest and NaCl solution addition. Operating variables are extraction time (20–180 min), material size (0.5, 1.0, and 1.5 cm), feed-to-solvent ratio (0.1; 0.15; and 0.2 g/mL), and microwave power (300, 450, and 600 watts). The essential oil results are analyzed by GC-MS analysis, specific gravity, refractive index, and solubility. The results showed that it increased with extraction time followed by almost constant conditions, tended to decrease with increasing feed-to-solvent ratio, and increased yield with increasing microwave power. The results from the GC-MS analysis, the active substance content of geraniol was 46.61% and citronellal 5.62%. Additional salt in this method is a green and clean essential oil extraction.
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来源期刊
Indonesian Journal of Chemistry
Indonesian Journal of Chemistry CHEMISTRY, MULTIDISCIPLINARY-
CiteScore
2.30
自引率
11.10%
发文量
106
审稿时长
15 weeks
期刊介绍: Indonesian Journal of Chemistry is a peer-reviewed, open access journal that publishes original research articles, review articles, as well as short communication in all areas of chemistry, including educational chemistry, applied chemistry, and chemical engineering.
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