探针超声法合成氧化锶纳米粒子的光催化活性及电化学传感器研究

K.B. Kusuma , M. Manju , C.R. Ravikumar , N. Raghavendra , T. Naveen Kumar , M.R. Anilkumar , H.P. Nagaswarupa , T.R. Shashi Shekhar , H.C. Ananda Murthy , K.U. Aravind
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引用次数: 4

摘要

在本文中,我们报道了使用一种新的探针超声处理方法合成氧化锶纳米颗粒(SONP)。利用粉末X射线衍射(PXRD)对制备的材料的物理化学性质进行了表征,证实了SrO的平均晶粒尺寸为43​nm。漫反射光谱(DRS)的Kubelka-Monk函数用于确认SONP的平均能隙(4.06​eV)。SONP已成功地与本发明的光催化剂结合用于去除染料,例如亚甲蓝(MB)和酸性绿(AG)。以MB和AG染料为标准染料,研究了纳米颗粒在紫外光和阳光下的光催化性能。这些纳米氧化物在暴露于紫外线时以显著的效率光降解亚甲基蓝(87.70%)和酸性绿(71.20%)染料。当在不同扫描速度的循环伏安法测试中使用对乙酰氨基酚作为分析物时,这些纳米氧化物表现出优异的灵敏度(10​mV/s至50​mV/s)。因此,SONP可用于光催化活性和电化学传感器应用。
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Synthesis of strontium oxide nanoparticlesby probe sonication method: Its photocatalytic activity and electrochemical sensor studies

In this paper, we report on the synthesis of strontium oxide nanoparticles (SONPs) using a novel probe sonication method. Powder X-ray diffraction (PXRD) was used to characterize the physicochemical properties of the prepared materials, which confirmed that the average SrO crystallite size was 43 ​nm. The Kubelka-Monk function of diffuse reflectance spectroscopy (DRS) was used to confirm the average energy gap of SONPs (4.06 ​eV). SONPs have been successfully used in conjunction with inventive photocatalysts to remove dyes such as Methylene Blue (MB) and Acid Green (AG). MBand AG dyes were used as standard dyes to investigate the photocatalytic properties of NPs when exposed to UV light and sunlight.These nanometal oxides photodegrade methylene blue (87.70%) and acid green (71.20%) dyes with remarkable efficiency when exposed to UV light. These nanometal oxides demonstrated superior sensitivity when paracetamol was used as an analyte in cyclic voltammetry tests at various scan speeds (10 ​mV/s to 50 ​mV/s). As a result, SONPs may be useful in photocatalytic activity and electrochemical sensor applications.

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