热固性聚合物合成锌纳米颗粒的显微研究

Q3 Immunology and Microbiology Applied Microscopy Pub Date : 2019-12-31 DOI:10.1186/s42649-019-0018-0

Giriraj Tailor, Jyoti Chaudhay, Deepshikha Verma, Bhupendra Kr. Sarma

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引用次数: 7

摘要

本文报道了用热分解法合成锌纳米颗粒(Zn NPs)的新方法，并通过扫描电镜(SEM)、透射电镜(TEM)和x射线衍射仪(XRD)对其进行了表征。以热固性聚合物和锌盐为前驱体，合成了锌纳米粒子。在850℃下煅烧得到Zn NPs。°C 30min。SEM研究表明，合成的纳米颗粒呈球形。XRD分析表明，形成的Zn NPs具有低晶性。

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Microscopic study of zinc nanoparticles synthesised using thermosetting polymer

The present study reports the novel synthesis of Zinc nanoparticles (Zn NPs) by thermal decomposition method and its characterisation by Scanning Electron Microscope (SEM), Transmission Electron Microscope (TEM), and X-ray Diffraction Measurements (XRD). Synthesis of Zn NPs was achieved by using thermosetting polymer and zinc salts as precursor. Zn NPs were obtained on calcination at 850?°C for 30?min. SEM study reveals that synthesized nanoparticles are spherical in shape. XRD analysis shows that the Zn NPs formed are low crystalline in nature.

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来源期刊

Applied Microscopy Immunology and Microbiology-Applied Microbiology and Biotechnology

CiteScore

3.40

自引率

0.00%

发文量

审稿时长

10 weeks

期刊介绍： Applied Microscopy is a peer-reviewed journal sponsored by the Korean Society of Microscopy. The journal covers all the interdisciplinary fields of technological developments in new microscopy methods and instrumentation and their applications to biological or materials science for determining structure and chemistry. ISSN: 22875123, 22874445.