基于新型光电探测器阵列的MAES分析仪光谱仪

Q4 Chemistry Analitika i Kontrol Pub Date : 2021-01-01 DOI:10.15826/analitika.2021.25.4.002
V. А. Labusov, A.V. Behterev, V. G. Garanin
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引用次数: 1

摘要

多通道发射光谱分析仪(MAES)作为600多个原子发射光谱分析系统的一部分在俄罗斯、独联体国家和其他国家的企业中运行。直到最近,MAES分析仪仅使用BLPP-369M1光电探测器阵列,其性能足以用于使用明亮的光谱激发源(例如电弧或火花放电)的整体原子发射光谱应用。为了解决高时空分辨率和高灵敏度的问题,基于两种新型光电探测器阵列- blpp -2000和BLPP-4000开发了高速MAES分析仪。VMK-Optoelektronika公司基于这些阵列开发并投入生产了许多光学光谱仪:原子发射光谱仪:Grand Globula和ekexpress电弧和火花光谱仪,用于通过石墨电极通道蒸发直接分析粉末和分析金属;洒注法快速分析粉末的Grand-Potok弧谱仪用于金属和合金快速分析的Grand-Ekspert和Favorit氩火花真空光谱仪;用于液体分析的Grand-SVCh微波诱导氮等离子体光谱仪和Grand-ISP电感耦合氩等离子体光谱仪;kolibrii - svch微波诱导空气等离子体光谱仪和Pavlin火焰原子发射光谱仪测定溶液中碱性和碱土元素。同时测定液体中元素的高分辨率连续源电热原子吸收光谱仪。
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Spectrometers with MAES analyzers based on new photodetector arrays
Multichannel analyzers of emission spectra (MAES) are operated as part of more than six hundred systems for atomic emission spectral analysis at enterprises in Russia, the CIS countries, and others. Until recently, MAES analyzers used only BLPP-369M1 photodetector arrays, whose performance is sufficient for integral atomic emission spectrometry applications using bright sources of spectral excitation based, for example, on an arc or spark electric discharge. To solve problems where high temporal spatial resolution and high sensitivity are required, high-speed MAES analyzers have been developed based on two new photodetector arrays—BLPP-2000 and BLPP-4000. A number of optical spectrometers based on these arrays have been developed and put into production by the VMK-Optoelektronika company: Atomic emission spectrometers: Grand Globula and Ekspress arc and spark spectrometers for the direct analysis of powders by evaporation from the channel of a graphite electrode and for the analysis of metals; Grand-Potok arc spectrometers for the rapid analysis of powders by the spill-injection method; Grand-Ekspert and Favorit argon-spark vacuum spectrometers for the rapid analysis of metals and alloys; Grand-SVCh microwave-induced nitrogen plasma spectrometers and Grand-ISP inductively-coupled argon plasma spectrometers for the analysis of liquids; Kolibri-SVCh microwave-induced air plasma spectrometers and Pavlin flame atomic emission spectrometers for the determination of alkaline and alkaline earth elements in solutions. Grand-AAS high-resolution continuous-source electrothermal atomic absorption spectrometers for the simultaneous determination of elements in liquids.
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来源期刊
Analitika i Kontrol
Analitika i Kontrol Chemistry-Analytical Chemistry
CiteScore
0.90
自引率
0.00%
发文量
15
期刊介绍: Analitika i Kontrol is a scientific journal covering theoretical and applied aspects of analytical chemistry and analytical control, published since autumn 1997. Founder and publisher of the journal is the Ural Federal University named after the first President of Russia Boris Yeltsin (UrFU, Ekaterinburg).
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